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决明子蒽醌提取方法的研究
引用本文:马云理,徐杰远.决明子蒽醌提取方法的研究[J].齐鲁药事,2004,23(7):41-42.
作者姓名:马云理  徐杰远
作者单位:1. 鲁南制药股份有限公司,临沂,275005
2. 临沂市药检所,临沂,276000
摘    要:目的 研究决明子蒽醌的提取方法。方法 以决明子总蒽醌含量为主要考察指标,对决明子的蒽醌类成分采用乙醇提取的方法,用正交设计法对影响提取工艺的因素进行了研究。结果 用 8倍量 5 0 %乙醇回流提取 1 5h,再加 6倍量5 0 %乙醇回流提取 1 5h,效果最好。结论 本试验为决明子蒽醌类成分的提取、富集和开发产提供了有义参考

关 键 词:决明子  蒽醌  正交实验  回流
文章编号:1672-7738(2004)07-0041-02

Research on extracting condition of anthraquinones in Semen cassiae
Ma Yun-li,Xu Jie-yuan.Research on extracting condition of anthraquinones in Semen cassiae[J].qilu pharmaceutical affairs,2004,23(7):41-42.
Authors:Ma Yun-li  Xu Jie-yuan
Affiliation:Ma Yun-li,Xu Jie-yuan 1
Abstract:Objective To research the extracting condition of anthraquinones in Semen cassiae.Methods Entire anthraquinones were used as main index during determination.The solvent was ethanol and orthogonal tests were carried out.Results Semen cassiae material was extracted twice with 50% ethanol in 1.5h,and the volume of solvent was about 8 times and 6 times of Semen cassiae material (mass) with refluxing separately.Conlusion This method was meaningful for extraction,enrichment and development of anthraquinones in Semen cassiae.
Keywords:Semen cassiae  anthraquinones constituents  orthogonal tests  refluxing
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