| 阔叶五层龙的化学成分研究 |
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| 引用本文： | 濮江,冯锋,郭青龙,谢宁.阔叶五层龙的化学成分研究[J].中国现代应用药学,2009,26(11):916-918. |
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| 作者姓名： | 濮江 冯锋 郭青龙 谢宁 |
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| 作者单位： | 1.中国药科大学天然药化教研室，南京210009；2.江苏省肿瘤发生与干预重点实验室，南京 210009 |
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| 摘 要： | 目的对阔叶五层龙所含化学成分进行研究。方法应用液-液萃取及多种柱层析方法进行化学成分的分离、纯化，并利用多种光谱技术进行结构的分析鉴定。结果从阔叶五层龙植物中分离得到9个化合物：2-hydroxyfriedelan-3-one (1)，软木三萜酮 (2), lup-20(29)-en-3, 21-dione (3)，D-friedoolean-14-en-3-one (4)，3-(3″,4″-dihydroxy-trans-cinnamoyloxy)-D- friedoolean-14-en-28-oic acid (5), 3, 22-dioxo-29-normoretane (6), 羽扇豆醇 (7), β-谷甾醇 (8), β-胡萝卜苷(9)。结论该9个化合物均为首次从阔叶五层龙中分离得到。
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| 关 键 词： | 牛蒡子 超临界CO2萃取 脱脂 均匀设计 GC-MS |
| 收稿时间： | 1/1/1900 12:00:00 AM |
Study on Chemical Constituents from Salacia amplifolia |
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| PU Jiang,FENG Feng,GUO Qinglong,XIE Ning.Study on Chemical Constituents from Salacia amplifolia[J].The Chinese Journal of Modern Applied Pharmacy,2009,26(11):916-918. |
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| Authors: | PU Jiang FENG Feng GUO Qinglong XIE Ning |
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| Affiliation: | 1.Department of Natural Medicinal Chemistry, China Pharmaceutical University, Nanjing 210009, China; 2.Key Laboratory of Carcinogesis and Intervention of Jiangsu Province, Nanjing 210009, China |
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| Abstract: | OBJECTIVE To study the optimum parameters of defatting technology of Fructus Arctii by the supercritical CO2 fluid and chemical constituents. METHODS Supercritical CO2 fluid extraction condition was selected by uniform design. The extraction pressure, ext |
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| Keywords: | Fructus Arctii supercritical CO2 extraction defatting uniform design GC-MS |
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