| 多指标综合评分法优选当归芍药散提取工艺 |
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| 引用本文： | 周瑜,陶春蕾,许钒,宋欣,王成业.多指标综合评分法优选当归芍药散提取工艺[J].中国实验方剂学杂志,2012,18(19):20-23. |
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| 作者姓名： | 周瑜 陶春蕾 许钒 宋欣 王成业 |
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| 作者单位： | 安徽省高等学校省级现代中药重点实验室,安徽中医学院药学院,合肥230038 |
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| 基金项目： | 国家自然科学基金面上项目(81173368);安徽省高校自然科学研究重点项目(KJ2010A213) |
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| 摘 要： | 目的:优选当归芍药散的提取工艺.方法:以芍药内酯苷、芍药苷、阿魏酸、23-乙酰泽泻醇B为评定指标,用多指标综合评分法进行数据处理,选取提取时间、提取次数、乙醇体积分数及乙醇用量为考察因素,采用正交试验优化提取条件.结果:最佳提取工艺为加8倍量75％乙醇回流提取2次,每次1.5h.结论:该提取工艺稳定、合理,有效成分提取率高.
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| 关 键 词： | 当归芍药散 芍药内酯苷 芍药苷 阿魏酸 23-乙酰泽泻醇B 正交试验 综合评分法 |
| 收稿时间： | 2012/5/24 0:00:00 |
Optimization of Extraction Technology for Danggui Shaoyao Powder by Multiple-index Comprehensive Scoring Method |
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| ZHOU Yu,TAO Chun-lei,XU Fan,SONG Xin and WANG Cheng-ye.Optimization of Extraction Technology for Danggui Shaoyao Powder by Multiple-index Comprehensive Scoring Method[J].China Journal of Experimental Traditional Medical Formulae,2012,18(19):20-23. |
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| Authors: | ZHOU Yu TAO Chun-lei XU Fan SONG Xin and WANG Cheng-ye |
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| Affiliation: | Anhui Province Key Laboratory of Modern Chinese Medicine, College of Pharmacy, Anhui College of Traditional Chinese Medicine, Hefei 230038, China;Anhui Province Key Laboratory of Modern Chinese Medicine, College of Pharmacy, Anhui College of Traditional Chinese Medicine, Hefei 230038, China;Anhui Province Key Laboratory of Modern Chinese Medicine, College of Pharmacy, Anhui College of Traditional Chinese Medicine, Hefei 230038, China;Anhui Province Key Laboratory of Modern Chinese Medicine, College of Pharmacy, Anhui College of Traditional Chinese Medicine, Hefei 230038, China;Anhui Province Key Laboratory of Modern Chinese Medicine, College of Pharmacy, Anhui College of Traditional Chinese Medicine, Hefei 230038, China |
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| Abstract: | Objective:To optimize extraction conditions of Danggui Shaoyao powder. Method:With the content of albiflorin,paeoniflorin,ferulic acid and 23-acetate alisol B as indexes,test data was handled by multiple-index comprehensive scoring method,orthogonal test was adopted in optimizing extraction technology with extraction time,extraction times,the concentration of ethanol and ethanol volume as factors. Result:Optimized extraction technology was:extracted 2 times with 8 times the amount of 75% ethanol,1.5 h per time. Conclusion:This optimized extraction technology was rational and stable with high yield of active components. |
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| Keywords: | Danggui Shaoyao powder albiflorin paeoniflorin ferulic acid 23-acetate alisol B orthogonal test multi-index comprehensive scoring method |
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