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| 清热祛风胶囊质量标准研究 | |
| 引用本文： | 王志刚,李双,葛红侠,杨洪武,徐涓.清热祛风胶囊质量标准研究[J].辽宁中医杂志,2008,35(7):1071-1072. |
| 作者姓名： | 王志刚 李双 葛红侠 杨洪武 徐涓 |
| 作者单位： | 1. 辽宁省医药工业研究院,辽宁,沈阳,110015 2. 辽宁天蜂实业股份有限公司,辽宁,沈阳,110027 3. 辽宁可济药业有限公司,辽宁,沈阳,110102 |
| 摘 要： | 目的:建立清热祛风胶囊的质量标准。方法:用薄层色谱法对处方中的冰片、黄连、青黛进行定性鉴别,用高效液相色谱法测定栀子苷的含量。结果:用TLC法能检出冰片、黄连、青黛;栀子苷进样量在250.8~752.4ng范围内与峰面积线性关系良好(r=0.9998);平均回收率分别为99.04%,RSD=1.03%(n=6)。结论:所用方法简便、准确、重现性好,能有效控制清热镇惊胶囊胶囊的质量。 |
| 关 键 词： | 清热祛风胶囊 栀子苷 薄层色谱法 高效液相色谱法 |
Study on the Quality Standard of Qingrequfeng Capsule |
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| WANG Zhi-gang,LI Shuang,GE Hong-xia,YANG Hong-wu,XU Juan.Study on the Quality Standard of Qingrequfeng Capsule[J].Liaoning Journal of Traditional Chinese Medicine,2008,35(7):1071-1072. | |
| Authors: | WANG Zhi-gang LI Shuang GE Hong-xia YANG Hong-wu XU Juan |
| Abstract: | Objective:To establish the quality standard for Qingrequfeng capsules.Methods:Borneol,Rhizoma Coptidis and Indigo Naturalis were identified by TLC,and the content of gardenoside was determined by HPLC.Results:Borneol,Rhizoma Coptidis and Indigo Naturalis could be identified by TLC.The determination of gardenoside showed a good linear relationship in the range of 250.8～752.4ng(r=0.9998).The average recovery was 99.04% with RSD of 1.03%(n=6).Conclusion:The method is simple,rapid and accurate.It can be used for quality control of Qingrequfeng capsules. |
| Keywords: | Qingrequfeng capsules gardenoside TLC HPLC |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |
