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中药材水半夏质量标准研究
引用本文:江秀娟,梁华伦,黄珊.中药材水半夏质量标准研究[J].亚太传统医药,2014(4):35-36.
作者姓名:江秀娟  梁华伦  黄珊
作者单位:[1]广州市海珠区食品药品检验所,广东广州510250 [2]广东省中医院,广东广州510515 [3]广州市岭南中药饮片有限公司,广东广州501000
摘    要:目的:研究水半夏的质量标准。方法:参考《中国药典》2010年版方法,对中药材水半夏的质量控制方法进行研究,包括显微鉴别、薄层色谱鉴别、水分检查、总灰分检查和浸出物检查。结果:10批水半夏测试样品中水分含量为11.4%~16.9%,平均值为14.0%;总灰分为4.7%~7.5%,平均值为6.0%;冷浸法水溶性浸出物量为5.4%~8.7%,平均值为6.9%,薄层色谱操作简便,结果准确、可靠,重现性好。结论:该实验制定的方法可应用于水半夏的质量控制。

关 键 词:水半夏  中药材  质量标准

Study on the Quality Standard of Rhizoma Typhonii Flagelliformis
Jiang Xiujuan,Liang Hualun,Huang Shan.Study on the Quality Standard of Rhizoma Typhonii Flagelliformis[J].Asia-Pacific Traditional Medicine,2014(4):35-36.
Authors:Jiang Xiujuan  Liang Hualun  Huang Shan
Affiliation:1. Food and Drug Inspection of Haizhu District of Guangzhou, Guangdong 510250,China: 2. Traditional Chinese Medicine Hospital of guangdong ,Guangdong 510515 ,China; 3. I.ingnan Herbal Pieces co. , I.TD of Guangzhou, Guangdong 501000. China)
Abstract:Objective:To establish and perfect the quality standard system of Rhizoma typhonii flagelliformis. Methods:The researches included microscopic identification ,TI.C discriminates, edematous amaenorrhea, total ashes, water-soluble extracts of the Rhizoma typhonii flagelliformis samples were investigated with the detemfination method in Chinese Pharmacopeoia published in 2010. Results: The edematous amaenorrhea were 11. ,t ~ ~ 16.9 ~, with an anavenage value of 14.0 %0 ;the total ashes were 4.7 ~7.5~,with an average volue of 6.0%.the water soluble extracts in hot water were5.4%-8. 7%, with an average value of 6.9 %. TLC of Rhizoma typhonii flagelliformis was simple, accurate, reliable and reproducible. Conclusion : Thin-layer chromatography identification, proprietary methods, clear spots. A complete set of quality standards has been formed.
Keywords:Rhizoma Typbonii Flagelliformis  Chinese Crude Drug  Quality Standard
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