| 枳实导滞浓缩丸质量标准研究 |
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| 引用本文： | 刘友平,宋英,秦春梅,张家明.枳实导滞浓缩丸质量标准研究[J].中国中药杂志,2002,27(11):838-840. |
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| 作者姓名： | 刘友平 宋英 秦春梅 张家明 |
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| 作者单位： | 1. 成都中医药大学,四川,成都,610075
2. 成都中医药大学,附属医院,四川,成都,610075 |
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| 摘 要： | 目的 :建立枳实导滞浓缩丸的质量标准。方法 :采用TLC对处方中的大黄、枳实、黄连、黄芩进行定性鉴别 ;用HPLC法测定方中君药大黄中大黄素的含量。结果 :在TLC色谱中 ,能检出大黄、枳实、黄连、黄芩 ;大黄素在 0.0612～0.6120μg与峰面积积分值呈良好的线性关系 ,r =0.9999,平均回收率 97.9% ,RSD =2.1%。结论 :所建立的方法对方中 4味药材能准确、快速地进行定性、定量检测 ,可用于枳实导滞浓缩丸的质量控制。
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| 关 键 词： | 枳实导滞浓缩丸 TLC HPLC 大黄素 |
| 文章编号： | 1001-5302(2002)11-0838-03 |
| 收稿时间： | 2002/3/29 0:00:00 |
| 修稿时间： | 2002年3月29日 |
Studies on Quality Control Standard of Zhishidaozhi Tabloid Pills |
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| LIU You-ping;SONG Ying;QIN Chun-mei;ZHANG Jia-ming.Studies on Quality Control Standard of Zhishidaozhi Tabloid Pills[J].China Journal of Chinese Materia Medica,2002,27(11):838-840. |
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| Authors: | LIU You-ping;SONG Ying;QIN Chun-mei;ZHANG Jia-ming |
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| Affiliation: | Chengdu University of TCM, Chengdu 610075, Sichuan, China. Liu-youping@msn.com |
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| Abstract: | OBJECTIVE: To develop the quality control standard of Zhishidaozhi Tabloid Pills. METHOD: Applying TLC to identify Radix et Rhizoma Rhei, Fructus Aurantii Immaturus, Rhizoma Coptidis, Radix Scutellariae, and HPLC to determine the content of emodin of Radix et Rhizoma Rhei. RESULT: Radix et Rhizoma Rhei, Fructus Aurantii Immaturus, Rhizoma Coptidis and Radix Scutellariae could be indentified by TLC. Emodin showed a good linear relationship at a rang of 0.0612-0.612 microgram, r = 0.9999. The average recovery was 97.9%, and RSD was 2.1%. CONCLUSION: The methods are accurate and quick, and can be used for the quality control of Zhishidaozhi Tabloid Pills. |
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| Keywords: | Zhishidaozhi Tabloid Pills TLC HPLC emodin |
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