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银杏内酯A、B和白果内酯的分离与纯化
引用本文:韩金玉,褚巧伟,常贺英,王华,王海静.银杏内酯A、B和白果内酯的分离与纯化[J].中草药,2000,31(9):652-653.
作者姓名:韩金玉  褚巧伟  常贺英  王华  王海静
作者单位:天津大学化工学院(300072)
基金项目:天津市自然科学基金项目(No.993606911)
摘    要:以银杏叶浸膏EGb761为原料,通过预处理,制备色谱和重结晶过程,得到纯度达98%以上的银杏内酯A、B和白果内酯纯品。建立了一种较简单的分离和纯化银杏内酯A、B和白果内酯的方法。

关 键 词:银杏内酯  白果内酯  制备色谱  预处理  重结晶
收稿时间:1999/11/2 0:00:00
修稿时间:1999年11月2日

Isolation and Purification of Ginkgolide A, B and Bilobalide
HanJinyu,Chu Qiaowei,Chang Heying,Wang Hua and Wang Haijing.Isolation and Purification of Ginkgolide A, B and Bilobalide[J].Chinese Traditional and Herbal Drugs,2000,31(9):652-653.
Authors:HanJinyu  Chu Qiaowei  Chang Heying  Wang Hua and Wang Haijing
Affiliation:Tianjin 300072
Abstract:A simple method for the isolation and purification of ginkgolide A, B and bilobalide (ginkgo terpene trialctone) was developed A commercially available extract of leaves of Ginkgo biloba L. containing >6% ginkgo terpene trilactone was used as the raw material After partition in EtOAc, the enriched extract was separated to give individual terpenes by preparative liquid chromatography Ginkgolide A, B and bilobalide could be isolated with high purity by recrystallizing in MeOH H 2O
Keywords:ginkgolide bilobalide preparative liquid chromatography
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