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固精片质量标准的研究
引用本文:王玉巧,陈鹏,熊莉.固精片质量标准的研究[J].中成药,2005,27(9):1027-1029.
作者姓名:王玉巧  陈鹏  熊莉
作者单位:湖北省暨武汉市中药现代化工程技术研究中心,湖北,武汉,430052
摘    要:目的:建立了固精片的质量标准(乳香、香附、木香等).方法:采用TLC法对处方中乳香、香附、木香进行鉴别;用HPLC法测定木香烃内酯的含量.结果:薄层斑点清晰,专属性强.含量测定线性关系良好,平均回收率为99.1%,RSD为1.25%(n=5).结论:该方法简便准确,重现性好,可作为该制剂的质量控制.

关 键 词:固精片  木香烃内酯  质量标准
文章编号:1001-1528(2005)09-1027-03
收稿时间:09 3 2004 12:00AM
修稿时间:2004-09-03

Quality standard for Gujing Tablets
WANG Yu-qiao,CHEN Peng,XIONG Li.Quality standard for Gujing Tablets[J].Chinese Traditional Patent Medicine,2005,27(9):1027-1029.
Authors:WANG Yu-qiao  CHEN Peng  XIONG Li
Abstract:AIM: To establish the quality standard for Gujing Tablets (Olibanum, Rhizoma Cyperi, Radix Aucklandia, etc.). METHODS: Olibanuln, Rhizoma Cyperi, Radix Aucklandia were identified by TLC, and costuslactone content in Radix Aucklandia was determined by HPLC. RESULTS: The TLC identification was highly specific and spots were clear. Costuslactone in Radix Aucklandia showed a good linear relationship. The average recovery was 99.1% (RSD=1.2% and n=5). CONCLUSION: The methods are simple, reliable and have a good reproducibility and can be used for the quality control of Gujing Tablets.
Keywords:TLC  HPLC
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