| 玉屏风口服液的质量标准研究 |
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| 引用本文： | 夏玉凤,杨勤,薛丽琼,王强.玉屏风口服液的质量标准研究[J].中成药,2003,25(12):967-970. |
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| 作者姓名： | 夏玉凤 杨勤 薛丽琼 王强 |
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| 作者单位： | 中国药科大学中药分析教研室,江苏,南京,210038 |
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| 摘 要： | 目的：建立玉屏风口服液(黄芪、防风、白术)的质量标准。方法：用薄层色谱法对黄芪、防风、白术进行了定性鉴别；用高效液相色谱—蒸发光散射检测器(HPLC—ELSD)法测定了口服液中黄芪甲苷的含量。结果：定性鉴别分离度好，专属性强：含量测定黄芪甲苷的平均加样回收率为97．75％，RSD为1．31％。结论：方法简便准确、灵敏度高，可用于玉屏风口服液的质量控制。
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| 关 键 词： | 玉屏风口服液 薄层色谱 黄芪甲苷 HPLC-ELSD |
| 文章编号： | 1001-1528(2003)12-0967-04 |
| 修稿时间： | 2003年6月16日 |
Study on quality standard of Yupingfeng Oral Liquid |
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| XIA Yu-feng,YANG Qin,XUE Li-qiong,WANG Qiang.Study on quality standard of Yupingfeng Oral Liquid[J].Chinese Traditional Patent Medicine,2003,25(12):967-970. |
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| Authors: | XIA Yu-feng YANG Qin XUE Li-qiong WANG Qiang |
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| Abstract: | Objective: To established a method for the quality standard of Yupingfeng Oral Liquid(Radix Astragali, Radix Saposhnikoviae and Rhizoma Atractylodis Macrocephalae). Methods:Radix Astragali, Radix Saposhnikoviae and Rhizoma Atractylodis Macrocephalae in oral liquid were identified by TLC. The content of astragaloside IV was determined by HPLC-ELSD. Results:The study showed that spots of samples on TLC can be well separated and the method had strong specificity. The average recovery was 97.75% and RSD was 1.31%. Conclusion:The method is simple, sensitive and accurate. It can be used for quality control of Yupingfeng Oral Liquid. |
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| Keywords: | Yupingfeng Oral Liquid TLC astragaloside IV HPLC |
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