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加压提取地榆根中黄酮成分的研究
引用本文:于慧荣,赵文英,朱兆友.加压提取地榆根中黄酮成分的研究[J].天然产物研究与开发,2011,23(3):449-452.
作者姓名:于慧荣  赵文英  朱兆友
作者单位:青岛科技大学化工学院,青岛,266042
基金项目:青岛科技大学科研启动基金资助,山东省中青年科学家科研奖励基金
摘    要:研究加压提取地榆中黄酮的最佳提取工艺。探讨了乙醇浓度、料液比、粒径、提取压力、提取温度和提取时间6个因素对黄酮得率的影响,并通过正交试验优化,确定了加压提取地榆中黄酮的最佳条件。结果表明加压提取地榆中黄酮的最佳提取条件:浸提温度120℃,料液比为1∶20,提取溶剂为60%的乙醇,浸提时间为30min,浸提压力为5 kg/cm2,粒径为40目,在该条件下黄酮提取率可达17.35%。与回流提取法相比,加压浸提法可显著提高浸提率。

关 键 词:地榆根  黄酮  加压提取

Extraction of Total Flavonoids from Sanguisorba officinalis Root by Pressurized Liquid Extraction
YU Hui-rong,ZHAO Wen-ying,ZHU Zhao-you.Extraction of Total Flavonoids from Sanguisorba officinalis Root by Pressurized Liquid Extraction[J].Natural Product Research and Development,2011,23(3):449-452.
Authors:YU Hui-rong  ZHAO Wen-ying  ZHU Zhao-you
Affiliation:YU Hui-rong,ZHAO Wen-ying,ZHU Zhao-you College of Chemical Engineering,Qingdao University of Science and Technology,Qingdao 266042,China
Abstract:The extraction process of flavonoids from Sanguisorba officinalis root using pressurized liquid extraction(PLE) was studied and compared with reflux extraction.Significant parameters affecting PLE procedure such as the concentration of ethanol,solid-liquid ratio, temperature,pressure,time,and material size were discussed and optimized by the orthogonal test.The results showed that the optimized conditions were as follows:the extraction solvent 60% ethanol water solution,the material size 40 mesh,ratio of ma...
Keywords:Sanguisorba officinalis root  Flavonoids  pressurized liquid extraction  
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