| 智能稀释DUO-ICP-AES测定密封不锈钢食品容器中铅、镉、铬、镍溶出量 |
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| 引用本文： | 钟志光,何颖贤,李政军,赵泉,郑建国,张遴,乐爱山.智能稀释DUO-ICP-AES测定密封不锈钢食品容器中铅、镉、铬、镍溶出量[J].润滑与密封,2009,34(10). |
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| 作者姓名： | 钟志光 何颖贤 李政军 赵泉 郑建国 张遴 乐爱山 |
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| 作者单位： | 1. 广东出入境检验检疫局,广东广州,510623
2. 陕西出入境检验检疫局,陕西西安,710068 |
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| 基金项目： | 国家公益性行业专项项目(10-72) |
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| 摘 要： | 采用智能稀释DUO-ICP-AES法测定密封不锈钢食品容器中铅、镉、铬、镍的溶出量,并对3%乙酸溶液中仪器的分析线选择、背景校正、入射功率、雾化器压力、辅助气流量、冷却气流量、蠕动泵转速的影响及共存元素的干扰等因素进行了研究。该方法的检测限为:铅0.0066mg/L;镉0.0009mg/L;铬0.0017mg/L;镍0.0011mg/L,其回收率和精密度分别为93.2%～99.4%和0.48%～2.3%。该方法快速简便,具有良好的精密度和准确度,适用于进出口密封不锈钢食品容器的日常检验。
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| 关 键 词： | 原子发射光谱 不锈钢容器 重金属 |
Study on Simultaneous Determination of Pb,Cd,Cr,Ni Leaching Quantity from Stainless Steel Sealed Food Containers by DUO-ICP-AES with Automatic Dilution Technique |
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| Zhong Zhiguang,He Yingxian,Li Zhengjun,Zhao Quan,Zheng Jianguo,Zhang Lin,Yue Aishan.Study on Simultaneous Determination of Pb,Cd,Cr,Ni Leaching Quantity from Stainless Steel Sealed Food Containers by DUO-ICP-AES with Automatic Dilution Technique[J].Lubrication Engineering,2009,34(10). |
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| Authors: | Zhong Zhiguang He Yingxian Li Zhengjun Zhao Quan Zheng Jianguo Zhang Lin Yue Aishan |
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| Affiliation: | 1.Guangdong Entry-Exit Inspection & Quarantine Bureau;Guangzhou Guangdong 510623;China;2.Shaanxi Entry-Exit Inspection & Quarantine Bureau;Xi'an Shaanxi 710068;China |
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| Abstract: | The method was developed for the simultaneous determination of Pb,Cd,Cr,Ni leaching quantity from stainless steel sealed food containers by dual observation-inductively coupled plasma atomic emission spectrometry with automatic dilution technique.The factors such as the selection of analytical wavelengths,the correction of the background,the influence of instrument parameters such as power,nebulizer pressure,auxiliary gas,peristaltic pump rate in 3% acetic acid,and the interference of coexistent elements we... |
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| Keywords: | atomic emission spectrometry stainless steel containers heavy metal |
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