微波法制备银镁共掺氧化锌复合光催化剂及其光催化性能研究 |
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引用本文: | 孙博,吴限,张金生,李丽华.微波法制备银镁共掺氧化锌复合光催化剂及其光催化性能研究[J].石油炼制与化工,2020,51(6):47-51. |
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作者姓名: | 孙博 吴限 张金生 李丽华 |
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作者单位: | 辽宁石油化工大学化学化工与环境学部 |
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摘 要: | 采用环形聚焦单模微波辅助法(简称微波法)快速合成银镁共掺氧化锌复合光催化剂(简称复合光催化剂),并运用X射线衍射、扫描电子显微镜对其结构和形貌进行表征。将此复合光催化剂应用于光催化降解罗丹明B和含油污水,研究其光催化性能并探究光催化降解机理。结果表明:微波法合成的复合光催化剂具有良好的光催化性能,对含油污水的降解率优于商用二氧化钛;复合光催化剂重复使用4次后罗丹明B的降解率仍维持在92%以上,化学稳定性良好。。
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关 键 词: | 微波法 氧化锌 光催化剂 含油污水 |
收稿时间: | 2019-12-26 |
修稿时间: | 2020-02-05 |
MICROWAVE-ASSISTED SYNTHESIS OF SILVER-MAGNESIUM CO-DOPED ZINC OXIDE AND ITS PHOTOCATALYTIC PERFORMANCE |
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Abstract: | A ring-focusing single-mode microwave synthesis method was used to rapidly synthesize a composite photocatalyst of silver-magnesium co-doped ZnO. XRD and SEM were used to characterize the structure and morphology of the synthesized photocatalyst. The photocatalytic degradation of Rhodamine B and oily wastewater by the photocatalyst was investigated. The performance and the mechanism of the reactions were explored. The results showed that the composite photocatalyst synthesized by microwave method had a good photocatalytic performance, and the degradation rate for oily wastewater was better than that of commercial titanium dioxide. After four cycles, the degradation rate of Rhodamine B was still above 92%, indicating that its chemical stability was good. |
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Keywords: | microwave method zinc oxide photocatalyst oily wastewater |
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