Synthesis of tin oxide-coated gold nanostars and evaluation of their surface-enhanced Raman scattering activities |
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Authors: | Aylin Elci Ozge Demirtas Ibrahim Murat Ozturk Alpan Bek Emren Nalbant Esenturk |
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Affiliation: | 1.Department of Chemistry,Middle East Technical University,Ankara,Turkey;2.Micro and Nanotechnology Program,Middle East Technical University,Ankara,Turkey;3.Department of Physics,Middle East Technical University,Ankara,Turkey |
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Abstract: | Tin oxide-coated gold nanostar hybrid nanostructures are prepared by first synthesizing gold nanostars (ca. 400 nm), then introducing Na2SnO3 precursor followed by its hydrolysis and formation of a tin oxide layer on nanoparticle surface. The synthesized hybrid structures have been characterized by combination of UV–Vis spectroscopy, transmission electron microscope (TEM), energy-dispersive X-ray studies, scanning electron microscope (SEM), X-Ray diffraction (XRD) and Fourier transform infrared (FTIR) spectroscopy. The TEM and SEM analyses showed that gold nanostars have a coating with an approximate thickness of 15 nm. The tin (IV) oxide coating on the gold nanostars was identified by XRD and XPS analyses and confirmed by FTIR spectroscopy. Surface-enhanced Raman scattering (SERS) spectroscopy was performed on tin oxide-coated and uncoated gold nanostars with crystal violet as a probe molecule. The SERS studies revealed field enhancement properties of Au nanostars, thus their strong SERS activity remained after tin oxide coating. |
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