| 硫酸软骨素光度分析方法的改进 |
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| 引用本文： | 伍茂云,谢书伸,冉蓉,李晓燕,王槐三,税德清.硫酸软骨素光度分析方法的改进[J].四川大学学报(工程科学版),2000,32(3):101-103. |
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| 作者姓名： | 伍茂云 谢书伸 冉蓉 李晓燕 王槐三 税德清 |
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| 作者单位： | 1. 四川大学,应用化学系,成都,610065
2. 成都市成华区环境监测站,成都,610043 |
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| 基金项目： | 国家自然科学基金资助项目 !3 96 70 71 7 |
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| 摘 要： | 对硫酸软骨素的水解和光度分析条件作了系统研究和筛选，优选出最佳水解条件３Ｍ盐酸和沸水浴中水解６０～８０分钟，水解液再按改进的乙酰丙酮－对二甲氨基苯甲醛法作光度分析，测定精确度较高，与原分析方法比较，操作简化，测定时间缩短一半。
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| 关 键 词： | 硫酸软骨素 光度分析 酸性粘多糖 测定 |
Study on the Improvement of the Photometric Analysis Process of Chondroitini Sulfas |
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| WU Mao-yun,XIE Shu-shen,RAN Rong,LI Xiao-yan,WANG Huai-san,SHUI De-qing.Study on the Improvement of the Photometric Analysis Process of Chondroitini Sulfas[J].Journal of Sichuan University (Engineering Science Edition),2000,32(3):101-103. |
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| Authors: | WU Mao-yun XIE Shu-shen RAN Rong LI Xiao-yan WANG Huai-san SHUI De-qing |
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| Abstract: | The conditions of the hydrolysis and photometric analysis of Chondroitini Sulfas were studied and screened systemly. Then, the hydrolysized solution was analysized by acetyla cetone-p-dimethylamino benzaldehyde photometric process. Results showed that the hydrolytie optimum conditions were 3M HCl and to be heated 70-80min by boiling water. This analytical process had high measurement accuracy and simple operation, comparison with the old one, which can also save half time. |
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| Keywords: | chondroitini Sulfas photometric Analysis improvement |
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