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高效液相色谱法在二元酸分析中的应用
引用本文:王春梅,范丹丹.高效液相色谱法在二元酸分析中的应用[J].合成技术及应用,2012,27(2):54-56.
作者姓名:王春梅  范丹丹
作者单位:中国石化抚顺石油化工研究院,辽宁抚顺,113001
摘    要:用高效液相色谱法分析丁二酸、戊二酸和己二酸的混合物,分析采用Waters-ODS色谱柱、4×150 mm色谱柱、紫外检测器,用含甲醇20%(V/V)的磷酸-磷酸二氢钾缓冲溶液为流动相。该方法与气相色谱法相比,具有样品不需预处理、操作简单、分析速度快等优点。

关 键 词:高效液相色谱  丁二酸  戊二酸  己二酸

The application of HPLC Method on adipic acid analysis
Wang Chunmei,Fan Dandan.The application of HPLC Method on adipic acid analysis[J].Synthetic Technology and Application,2012,27(2):54-56.
Authors:Wang Chunmei  Fan Dandan
Affiliation:(Fush Research Institute of Petroleum and Petrochemical,SINOPEC,Liaoning Fushun 113001,China)
Abstract:The mixture of succinic acid,glutaric acid and adipic acid was analyzed by HPLC method which employed Waters-ODS chromatographic column,4×150 mm chromatographic column,UV detector and H3PO4-KH2PO4 buffer with 20%(v/v) methanol as mobile phase.Compared with GC method,this method has several advantages,such as no need for sample pretreatment,simple manipulation and time-saving analysis.
Keywords:HPLC  succinic acid  glutaric acid  adipic acid
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