| 微波法合成2H-[1,4]噁唑嗪基[2,3,4]喹啉-6-羧酸衍生物的方法研究 |
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| 引用本文： | 茹婷婷,丁晓岩.微波法合成2H-[1,4]噁唑嗪基[2,3,4]喹啉-6-羧酸衍生物的方法研究[J].化工时刊,2014(1):15-17. |
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| 作者姓名： | 茹婷婷 丁晓岩 |
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| 作者单位： | [1]吉林建筑大学,吉林长春130118 [2]通化市东昌区江东乡中心小学,吉林通化134000 |
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| 摘 要： | 介绍了一种操作比较简单、反应高效清洁的微波辅助合成喹啉内酯化合物的新方法。采用微波加热的方式,高产率的合成了一系列新型噁唑嗪基2,3,4]喹啉-6-羧酸衍生物,并且所合成得到的化合物都经过了红外光谱、核磁氢谱和质谱表征。
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| 关 键 词： | 微波法 喹啉类化合物 有机合成 |
A Method for Synthesis of 2H-[1,4] Oxazole Triazine [2,3,4] 6-Quinoline Carboxylic Acid Derivatives by Microwave |
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| Ru Tingting Ding Xiaoyan.A Method for Synthesis of 2H-[1,4] Oxazole Triazine [2,3,4] 6-Quinoline Carboxylic Acid Derivatives by Microwave[J].Chemical Industry Times,2014(1):15-17. |
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| Authors: | Ru Tingting Ding Xiaoyan |
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| Affiliation: | Ru Tingting Ding Xiaoyan(Department of Basic Sciences, Jilin Institute of Architecture and Civil Engineering, Jilin Changchun 130115; Dongchang District Jiangdong Central Primary School, Jilin Tonghua 134000) |
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| Abstract: | The new method was introduced for synthesis of quinolinelaetone compounds by microwave. The reac- tion was simple , high efficient and clean . Using the microwave heating, a series of oxazoletriazine 2,3,4] -6 - quinoline carboxylic acid derivatives were synthesized, and the compounds were characterizad by IR, 1H NMR and mass spectrometry. |
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| Keywords: | ~ Somicrowave qumohne organic synthesis |
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