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| 异喹啉及其同系物的分离 | |
| 引用本文： | 周霞萍,王德龙,何衍庆,王大方,王为国,吕苗,张海平,周杰,李乃民.异喹啉及其同系物的分离[J].过程工程学报,2003,3(3):274-277. |
| 作者姓名： | 周霞萍 王德龙 何衍庆 王大方 王为国 吕苗 张海平 周杰 李乃民 |
| 作者单位： | 1. 华东理工大学能源化工系,上海,200237 2. 华东理工大学自动控制系,上海,200237 3. 宝钢化工技术中心,上海,200942 |
| 摘 要： | 以喹啉残油为原料, 通过改性丝光沸石填料和金属丝网(孔板)填料增加异喹啉及其同系物分离时的物性差异，并通过设定、调节PID参数，考察不同条件下自整定控制对实验的影响. 结果表明：在自制的容积为3 L的半自动精馏装置中，利用功能填料由PID控制可以得到总收率80%~ 85%、纯度95%~98%的喹啉、异喹啉，甲基喹啉. |
| 关 键 词： | 异喹啉及其同系物 同分异构体 填料 PID自整定控制 |
| 文章编号： | 1009-606X(2003)03-0274-04 |
| 修稿时间： | 2002年10月30 |
Separation of Isoquinoline and Its Homologue |
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| ZHOU Xia-ping,WANG De-long,HE Yan-qing,WANG Da-fang,WANG Wei-guo,LU Miao,ZHANG Hai-ping,ZHOU Jie,LI Nai-min.Separation of Isoquinoline and Its Homologue[J].Chinese Journal of Process Engineering,2003,3(3):274-277. | |
| Authors: | ZHOU Xia-ping WANG De-long HE Yan-qing WANG Da-fang WANG Wei-guo LU Miao ZHANG Hai-ping ZHOU Jie LI Nai-min |
| Affiliation: | ZHOU Xia-ping1,WANG De-long1,HE Yan-qing2,WANG Da-fang2,WANG Wei-guo2,LU Miao3,ZHANG Hai-ping3,ZHOU Jie3,LI Nai-min3 |
| Abstract: | With quinoline resid as raw material, the influence of PID control on the experimental result under different conditions was evaluated by configuring PID parameters and amplifying properties difference between isoquinoline and its homologue through the use of modified mordenite and metal wire mesh fillings. The result of experiment shows that it is able to obtain quinoline and isoquinoline whose yields range from 80% to 85% and purity ranges from 95% to 98% in the self-made 3 L semi-auto rectification equipment. |
| Keywords: | isoquinoline and its homologue isomer filling PID |
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