| 界面聚合PANI掺杂工艺的研究 |
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| 引用本文： | 宋宝寅,王东红,马富花.界面聚合PANI掺杂工艺的研究[J].化学推进剂与高分子材料,2011,9(1):81-83. |
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| 作者姓名： | 宋宝寅 王东红 马富花 |
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| 作者单位： | 1. 太原科技大学材料科学与工程学院,山西太原,030024;中国电子科技集团公司第三十三研究所,山西太原,030006
2. 中国电子科技集团公司第三十三研究所,山西太原,030006 |
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| 基金项目： | 中国电子科技集团第33所所控基金 |
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| 摘 要： | 采用界面聚合法制备聚苯胺(PANI),通过正交设计重点考察过硫酸铵滴加完毕后搅拌时间、搅拌速度、HCl的掺杂时间和后期干燥时间4个因素对PANI掺杂程度和表面电阻的影响.结果表明4个因素对PANI表面电阻具有较大影响,其中搅拌时间影响最为显著,其次是干燥时间、HCI的掺杂时间,搅拌速度影响最小.在150r/min低速搅...
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| 关 键 词： | 导电聚苯胺 正交设计 界面聚合 制备工艺 |
Study on PANI Doping Process Through Interfacial Polymerization |
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| SONG Baoyin,WANG Donghong,MA Fuhua.Study on PANI Doping Process Through Interfacial Polymerization[J].Chemical Propellants & Polymeric Materials,2011,9(1):81-83. |
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| Authors: | SONG Baoyin WANG Donghong MA Fuhua |
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| Affiliation: | SONG Baoyin1,2,WANG Donghong2,MA Fuhua2(1.College of Materials Science and Engineering,Taiyuan University of Science and Technology,Taiyuan 030024,China,2.The 33th Institute of China Electronics Technology Group Corporation,Taiyuan 030006,China) |
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| Abstract: | The polyaniline(PANI) was prepared by interfacial polymerization method.The influence of four factors such as stirring time after dropping off ammonium persulfate(APS),stirring speed,HCl doping time and later drying time on PANI doping degree and surface resistance was mainly investigated by using orthogonal design.The results show that they all can remarkably influence on PANI surface resistance.The influence of the stirring time is the most significant among them,followed by drying time and HCl doping tim... |
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| Keywords: | conductive polyaniline orthogonal design interfacial polymerization preparation process |
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