| 新型磷—氮阻燃剂三(5,5-二甲基-1,3-二氧-2-磷杂环己烷-2-氧甲基)胺的合成及应用 |
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| 引用本文： | 高富业,欧育湘.新型磷—氮阻燃剂三(5,5-二甲基-1,3-二氧-2-磷杂环己烷-2-氧甲基)胺的合成及应用[J].精细化工,1998(2). |
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| 作者姓名： | 高富业 欧育湘 |
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| 作者单位： | 北京理工大学国家阻燃材料实验室 |
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| 摘 要： | 叙述了三（５，５ 二甲基 １，３ 二氧 ２ 磷杂环己烷 ２ 氧甲基）胺的合成方法。用元素分析、ＩＲ、１ＨＮＭＲ验证了化合物的结构，分析了除水剂、催化剂等反应条件对反应结果的影响。在聚氨酯软泡中的应用表明，该阻燃剂具有良好的阻燃性
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| 关 键 词： | 阻燃剂，三（5`5-二甲基-1`3-二氧-2-磷杂环己烷-2-氧甲基）胺，聚氨酯软泡 |
Synthesis and Application of Novel Phosphorous Nitrogen Containing Flame Retardant Tris(5,5-dimethyl-1,3-dioxa-2-phosphacyclohexane-2-oxymethyl)amine |
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| Abstract: | In this paper,the synthetic procedure of tris(5,5-dimethy-1,3-dioxa-2-phosphacyclohexane-2-oxymethyl)amine is described in detail.The structure of the obtained flame retardant was identified by IR,1HNMR and elementary analysis.In addition,the effects of water-trapping agent and catalyst on the reaction are discussed.The results of flame retardancy of flame retardant flexible polyurethane foam is promising. |
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| Keywords: | flame retardant tris(5 5-dimethyl-1 3-dioxa-2-phosphacyclohexane-2-oxymethyl)amine flexible polyureth ane foam |
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