| 常温固相反应合成纳米氧化锌 |
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| 引用本文： | 张永康,刘建本,易保华,陈德根,肖卓炳,陈上.常温固相反应合成纳米氧化锌[J].精细化工,2000,17(6):343-344,355. |
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| 作者姓名： | 张永康 刘建本 易保华 陈德根 肖卓炳 陈上 |
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| 作者单位： | 1. 吉首大学,生命科学与化学学院,湖南,吉首,416000
2. 湘西州外贸化工厂,湖南,吉首,416000 |
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| 基金项目： | 湖南省自然科学基金资助项目!(99ZZY2071) |
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| 摘 要： | 以ZnSO4·7H2 O和Na2 CO3 为原料 ,用室温固相化学反应首先合成出粒径为 12 7nm的前驱体碳酸锌 ,然后在 2 0 0℃热分解 ,经纯化后得到纳米氧化锌。经XRD和TEM检测 ,粒径为 6 0～12 .7nm。
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| 关 键 词： | 纳米氧化锌 固相反应 前驱体 |
Preparation of Nanocrystalline Zinc Oxide by Solid State Reaction at Room Temperature |
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| ZHANG Yong-kang,LIU Jian-ben,YI Bao-hua,CHEN De-gen,XIAO Zhuo-bing,CHEN Shang.Preparation of Nanocrystalline Zinc Oxide by Solid State Reaction at Room Temperature[J].Fine Chemicals,2000,17(6):343-344,355. |
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| Authors: | ZHANG Yong-kang LIU Jian-ben YI Bao-hua CHEN De-gen XIAO Zhuo-bing CHEN Shang |
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| Abstract: | Using ZnSO\-4·7H\-2O and Na\-2CO\-3 as raw materials,precursor (ZnCO\-3) with size distribution of 127 nm was synthesized by solidphase reaction at room temperature.Nanocrytalline ZnO was obtained by decomposing the precursor at 200 ℃and then washing with deionized water to remove impurities.Nanosized zinc oxide was characterized by Xray powder diffraction(XRD) and transmisson electron microscope (TEM).XRD and TEM showed that the crystalline ZnO was spherical particles with hexagonal structure and had uniform size distribution of 60～12.7 nm. |
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| Keywords: | nanocrystalline zinc oxide solid state reaction precursor |
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