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负载硫化镉的碳纳米管载镉量分析
引用本文:唐文华,邹洪涛,刘吉平,邹勇.负载硫化镉的碳纳米管载镉量分析[J].化学试剂,2006,28(7):417-418,428.
作者姓名:唐文华  邹洪涛  刘吉平  邹勇
作者单位:1. 北京理工大学,材料科学与工程学院,北京,100081;凯里学院,化学系,贵州,凯里,556000
2. 北京理工大学,材料科学与工程学院,北京,100081;黔南民族师范学院化学系,贵州,都匀,558000
3. 北京理工大学,材料科学与工程学院,北京,100081
基金项目:国防基础研究(J1500E002)资助项目。
摘    要:经高温灰化法预处理后用配位滴定分析法测定负载硫化镉的碳纳米管(CdS/CNTS)的载镉量,测试数据可靠准确,表明制备负载硫化镉碳纳米管催化剂时所加入的镉并不全部吸附在碳纳米管上,载镉效率随着碳纳米管载镉量的增加而降低。

关 键 词:碳纳米管  载镉量  高温灰化  配位滴定法  测定
文章编号:0258-3283(2006)07-0417-02
收稿时间:2005-12-11
修稿时间:2005-12-11

Determination of cadmium in CdS loaded carbon nanotube
TANG Wen-hua,ZOU Hong-tao,LIU Ji-ping,ZOU Yong.Determination of cadmium in CdS loaded carbon nanotube[J].Chemical Reagents,2006,28(7):417-418,428.
Authors:TANG Wen-hua  ZOU Hong-tao  LIU Ji-ping  ZOU Yong
Affiliation:1 . School of Material Science and Engineering, Beijing Institute of Technology, Beijing 100081, China; 2. Department of Chemistry, College of Kaili, Kaili 556000, China; 3. Qiannan Normal College of Nationalities, Duyun 558000, China
Abstract:With preconditioning by high temperature dry ashing method,the cadmium in CdS loaded carbon nanotube was determined by complexometric titration.Accurate and reliable analysis results were obtained.The result indicated that the amount of cadmium added in carbon nanotube was not adsorbed completely in carbon nanotube,the loading efficiency decreased with the increase of loading amount in the carbon nanotube.
Keywords:carbon nanotube  amount of cadmium supported  high temperature dry ashing  complexometric titration  determination
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