| HPLC法检测中药洗发水中阿魏酸的含量 |
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| 引用本文： | 任杰麟,张榕文,黄春静,万玉华,吴志强.HPLC法检测中药洗发水中阿魏酸的含量[J].香料香精化妆品,2013(2):52-55. |
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| 作者姓名： | 任杰麟 张榕文 黄春静 万玉华 吴志强 |
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| 作者单位： | 霸王(广州)有限公司,广东广州,510440 |
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| 基金项目： | 广州市白云区科技计划扶持资金项目 |
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| 摘 要： | 建立了一种中药洗发水中阿魏酸含量的检测方法。采用高效液相色谱法，通过单因素考察，筛选出提取洗发水中阿魏酸成分的最佳条件，并通过正交设计试验，确定最佳提取工艺。结果发现，洗发水中阿魏酸的最佳提取工艺为：料液比为1：7，溶剂为100％乙醇，超声提取时间为10min。在此条件下，洗发水中阿魏酸的提取含量最高。本方法为检测当归洗发水中有效成分的含量提供了依据。
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| 关 键 词： | 当归洗发水 高效液相色谱法提取工艺 正交设计 |
Study on the Content of Ferulic Acid from the Angelica sinensis in Herbal Shampoo by HPLC Method |
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| REN Jielin
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ZHANG Rongwen
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HUANG Chunjing
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WAN Yuhua
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WU Zhiqiang.Study on the Content of Ferulic Acid from the Angelica sinensis in Herbal Shampoo by HPLC Method[J].Flavour Fragrance Cosmetics,2013(2):52-55. |
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| Authors: | REN Jielin ZHANG Rongwen HUANG Chunjing WAN Yuhua WU Zhiqiang |
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| Affiliation: | ( BAWANG ( Guangzhou) Co. Ltd. ,Guangzhou 510440,Guangdong,China) |
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| Abstract: | To establish a method to detect the content of ferulic acid from the Angelica snensis in herbal shampoo, the optimum extracting method for Angelica sinensis in shampoo with HPLC was studied through single factor experiment and orthogonal design. The optimum extraction conditions were： the ratio of feedstock to solvent was 1/7, 100% ethanol was used as solvent, ultrasonic extraction time was 10 min. Under these conditions, the highest content of ferulic acid was obtained from herbal shampoo with Angelica sinensis. The result provided a reference for detecting the content of valuable actives in sample with Angelica sinensis. |
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| Keywords: | shampoo with Angelica sinensis HPLC extraction process orthogonal design |
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