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Optimisation of the spark plasma sintering process for high volume fraction SiCp/Al composites by orthogonal experimental design
Authors:Pengchao Kang  Qiqi Zhao  Shiqi Guo  Wei Xue  Hao Liu  Zhenlong Chao  Longtao Jiang  Gaohui Wu
Abstract:Based on orthogonal experimental design (OED), the effects of the sintering pressure, sintering temperature and holding time on the mechanical properties of 50 vol% silicon carbide particle (SiCp)/2024Al composites prepared by spark plasma sintering (SPS) were investigated. The sintering pressure had the greatest effect on the density and bending strength of the material among these three factors, followed by sintering temperature and holding time. The optimised process conditions for producing the 50 vol% SiCp/2024Al were sintering at 550 °C for 5 min under 40 MPa, which resulted in a composite material with a density of 99.7% and good interface bonding with a comparatively high bending strength of 766.65 MPa. This work provides a promising method to produce high volume fraction composites that can meet high strength requirements.
Keywords:Spark plasma sintering  Orthogonal experimental design  SiCp/2024Al  Mechanical properties
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