| 6-羟基-2-氟-N-取代芳基苄胺类化合物的合成 |
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| 引用本文： | 姚巍,付庆,郁林军,龚启孙.6-羟基-2-氟-N-取代芳基苄胺类化合物的合成[J].浙江化工,2005,36(11):13-14. |
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| 作者姓名： | 姚巍 付庆 郁林军 龚启孙 |
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| 作者单位： | 1. 国家南方农药创制中心浙江基地,浙江,杭州,310023
2. 浙江工业大学农药研究所,浙江,杭州,310014 |
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| 摘 要： | 6-羟基-2-氟-N-取代芳基苄胺类化合物是合成含氟嘧啶氧苄胺类除草剂的关键中间体,本文以2,6-二氟苯醛为起始原料,合成6-羟基-2-氟苯甲醛,再与芳胺缩合成Schiff 碱,最后经硼氢化钠还原,合成了5个化合物,其结构经1HNMR和MS表征.
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| 关 键 词： | 6-羟基-2-氟-N-取代芳基苄胺 6-羟基-2-氟苯甲醛 合成 |
Study on the Synthesis of the Herbicide of Pyrimidinyloxybenzylamine Derivatives |
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| YAO Wei,FU Qing,YU Lin-jun,GONG Qi-sun.Study on the Synthesis of the Herbicide of Pyrimidinyloxybenzylamine Derivatives[J].Zhejiang Chemical Industry,2005,36(11):13-14. |
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| Authors: | YAO Wei FU Qing YU Lin-jun GONG Qi-sun |
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| Abstract: | 2-Fluoro-6-hydroxy-N-substitutedaryl benzylamine derivatives are the key intemediates of the pyrimidinyloxybenzylamine herbicides,which were synthesized by using 2,6-difluorobenzaldehyde as starting material and by single hydroxidation,imination,deoxidization.5 Novel compounds were synthesized,and their structure were confirmed by 1H NMR and MS. |
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| Keywords: | 2-Fluoro-6-hydroxy-N-substitutedarylbenzylamine 2-Fluoro-6-hydroxybenzaldehyde synthesis |
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