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脱醇型室温硫化硅橡胶的制备
引用本文:朱洪江,刘彬,谢志坚,王强,毛云忠,周远建.脱醇型室温硫化硅橡胶的制备[J].有机硅材料,2022(1):38-41.
作者姓名:朱洪江  刘彬  谢志坚  王强  毛云忠  周远建
作者单位:中蓝晨光化工研究设计院有限公司
摘    要:以α,ω-二羟基聚二甲基硅氧烷为基胶,氨基硅烷JT-908为封端剂,添加气相法二氧化硅、交联剂、硅烷偶联剂和催化剂制得脱醇型室温硫化硅橡胶,研究了封端剂和气相法二氧化硅用量、催化剂种类和用量、硅烷偶联剂种类对硅橡胶性能的影响.结果表明,封端剂的较佳用量为4份,气相法二氧化硅的较佳用量为10份,催化剂选择二月桂酸二丁基锡...

关 键 词:脱醇型  封端剂  室温硫化  硅橡胶

Preparation of Dealcoholized RTV-1 Silicone Rubber
ZHU Hong-jiang,LIU Bin,XIE Zhi-jian,WANG Qiang,MAO Yun-zhong,ZHOU Yuan-jian.Preparation of Dealcoholized RTV-1 Silicone Rubber[J].Silicone Material,2022(1):38-41.
Authors:ZHU Hong-jiang  LIU Bin  XIE Zhi-jian  WANG Qiang  MAO Yun-zhong  ZHOU Yuan-jian
Affiliation:(China Bluestar Chengrand Co.,Ltd.,Chengdu 610041,Sichuan)
Abstract:Usingα,ω-dihydroxy polydimethylsiloxane(107 silicone rubber)as the base material,aminosilane JT-908 as the end-capping agent,adding fumed silica,cross-linking agent and silane coupling agent,the dealcoholized RTV silicone rubber was prepared.the effects of the amount of end-capping agent and fumed silica,the type and amount of catalyst,and the type of silane coupling agent on the properties of the silicone rubber were studied.The results show that the preferred end-capping agent is 4 phr,the fumed silica is 10 phr,the preferned catalyst of dibutyltin dilaurate is 0.1 phr,the silane coupling agent isγ-aminopropyltriethoxysilane.The silicone rubber prepared under the above conditions has a surface dry time of 15 min,a Shore hardness of 24 A,a tensile strength of 1.41 MPa,an elongation at break of 362%,and a shear strength of 1.38 MPa.
Keywords:dealcohol type  end-capping agent  room temperature vulcanization  silicone rubber
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