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合成聚硅酸硼镁硫酸铁的正交实验研究
引用本文:史继斌,许兴友,李树安,宋长生,胡文娟.合成聚硅酸硼镁硫酸铁的正交实验研究[J].环境工程学报,2009,3(1):81-84.
作者姓名:史继斌  许兴友  李树安  宋长生  胡文娟
作者单位:淮海工学院化学工程学院,连云港,22005
基金项目:江苏省教育厅重大基础研究项目(07KJA15011);江苏省普通高等学校“青蓝工程”学术带头人项目(2007);淮海工学院科研基金资助项目(2008)
摘    要:研究了用硅酸钠、硼砂、硫酸镁和硫酸铁为原料,制备聚硅酸硼镁硫酸铁(PSBMFS)混凝剂的方法及合成条件。通过正交实验,考查了硅酸活化pH值、缩聚反应时间和陈化时间等合成条件;同时考察了B/Si摩尔比、Mg/Si摩尔比和Fe/Si摩尔比等影响因素。结果表明:PSBMFS具有良好的混凝性能和脱色效果,能有效去除印染废水中的色度和COD,2种污染因子的去除率分别可达95.9%和67.9%。

关 键 词:聚硅酸硼镁硫酸铁  混凝剂  正交实验  印染废水

Study on synthesis of poly-silicic-boracic-magnesic-ferric sulfate by perpendicular experiment
Shi Jibin,Xu Xingyou,Li Shuan,Song Changsheng and Hu Wenjuan.Study on synthesis of poly-silicic-boracic-magnesic-ferric sulfate by perpendicular experiment[J].Techniques and Equipment for Environmental Pollution Control,2009,3(1):81-84.
Authors:Shi Jibin  Xu Xingyou  Li Shuan  Song Changsheng and Hu Wenjuan
Affiliation:School of Chemical Engineering,Huaihai Institute of Technology, Lianyungang 222005,School of Chemical Engineering,Huaihai Institute of Technology, Lianyungang 222005,School of Chemical Engineering,Huaihai Institute of Technology, Lianyungang 222005,School of Chemical Engineering,Huaihai Institute of Technology, Lianyungang 222005 and School of Chemical Engineering,Huaihai Institute of Technology, Lianyungang 222005
Abstract:The synthetic conditions and methods of poly-silicic-boracic-magnesic-ferric sulfate (PSBMFS) flocculant using sodium silicate, borax, bitter salt and ferric sulphate as raw materials were studied. pH of silicic acid activating, polycondensation time, ageing time, B-to-Si mol ratio, Mg-to-Si mol ratio and Fe-to-Si mol ratio were researched. The result indicates that PSBMFS has the fine flocculation and color removal performance, and can remove the colority and COD of dyeing wastewater effectively, the removal rates of the colority and COD can reach 95.9% and 67.9%, respectively.
Keywords:PSBMFS  flocculant  perpendicular experiment  dyeing wastewater  
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