| 一种毛细管内壁生长金膜的化学镀法 |
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| 引用本文： | 李巧霞,王金意,黄贝贝,霍胜娟,徐群杰,蔡文斌.一种毛细管内壁生长金膜的化学镀法[J].复旦学报(自然科学版),2009,48(1). |
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| 作者姓名： | 李巧霞 王金意 黄贝贝 霍胜娟 徐群杰 蔡文斌 |
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| 作者单位： | 李巧霞,徐群杰,LI Qiao-xia,XU Qun-jie(上海电力学院上海高校电力腐蚀控制与应用电化学重点实验室,上海,200090);王金意,黄贝贝,霍胜娟,蔡文斌,WANG Jin-yi,HUANG Bei-bei,HUO Sheng-juan,CAI Wen-bin(复旦大学化学系,上海,200433)
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| 基金项目： | 国家自然科学基金，上海电力学院科研基金 |
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| 摘 要： | 种子生长化学沉积法被用于制备玻璃毛细管内擘上金膜:在玻璃毛细管内壁自组装上氨基硅烷,然后利用静电相互作用组装上单层金溶胶纳米粒子,最后在管内缓慢注入含有氯金酸和盐酸羟胺化学镀液生长金薄膜.该方法通用易行,可在不同大小和形状的玻璃毛细管内壁形成厚度连续、均匀和可控的金属层.
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| 关 键 词： | 毛细管内壁 种子生长化学沉积 Au溶胶 Au薄膜 |
A Chemical Deposition for the Formation of Metallic Films on the Inner Wall of a Glass Capillary |
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| LI Qiao-xia,WANG Jin-yi,HUANG Bei-bei,HUO Sheng-juan,XU Qun-jie,CAI Wen-bin.A Chemical Deposition for the Formation of Metallic Films on the Inner Wall of a Glass Capillary[J].Journal of Fudan University(Natural Science),2009,48(1). |
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| Authors: | LI Qiao-xia WANG Jin-yi HUANG Bei-bei HUO Sheng-juan XU Qun-jie CAI Wen-bin |
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| Affiliation: | 1.Key Laboratory of Shanghai Colleges and Universities for Electric Power Corrosion Control and Applied Electrochemistry;Shanghai University of Electric Power;Shanghai 200090;China;2.Department of Chemistry;Fudan University;Shanghai 200433;China |
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| Abstract: | A seeded-growth chemical deposition was extended to form a continuous gold film onto the inner wall of a glass capillary,in which amino silane was first assemble onto the inner wall surface,then a monolayer of Au colloids was glued to the modified surface,and eventually a plating bath containing chloroauric acid and hydroxylamine was injected.This protocol is simple and general for fabricating thickness tunable,homogeneous and conductive metal films on the inner walls of capillaries of various shapes and si... |
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| Keywords: | glass capillary seeded-growth chemical deposition Au colloid Au film |
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