Studies on structural and electrical properties of Co1−xNixFe1.9Mn0.1O4 ferrite |
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Authors: | PA Shaikh RC Kambale AV Rao YD Kolekar |
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Affiliation: | aComposite Materials Laboratory, Department of Physics, Shivaji University, Kolhapur 416004, Maharashtra, India;bDepartment of Physics, University of Pune, Ganeshkhind, Pune 411007, (M.S.), India |
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Abstract: | Nickel-doped iron-deficient cobalt ferrite with small amount of manganese having the chemical composition Co1−xNixFe1.9Mn0.1O4, with x = 0.2, 0.4, 0.6 and 0.8, were prepared by standard double sintering ceramic method. The spinel phase formation was confirmed by X-ray diffraction (XRD). The DC resistivity measurements with temperature indicate a semiconducting behavior showing a linear decrease with increasing temperature and the doping of Ni enhances the resistivity. Maximum resistivity of the order of 109 Ω cm was found for composition x = 0.8. Room temperature dielectric constant measurements with frequency (100 Hz to 1 MHz), show usual dielectric dispersion. Also, the variation of room temperature AC conductivity as a function of frequency were studied and explained by using Maxwell–Wagner two-layer model. The studies on dielectric constant ( ′), loss tangent (tan δ) and AC conductivity (σAC), at four different frequencies (viz., 1, 10, 100 kHz and 1 MHz), with temperature were made. |
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Keywords: | Magnetically ordered materials Powder metallurgy Crystal structure and symmetry X-ray diffraction Electronic transport |
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