| 皮革中邻苯二甲酸酯的快速筛选——离子迁移谱法 |
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| 引用本文： | 吴泽颖,柳海军,朱珺,徐菽婧.皮革中邻苯二甲酸酯的快速筛选——离子迁移谱法[J].四川皮革,2014(18):35-38. |
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| 作者姓名： | 吴泽颖 柳海军 朱珺 徐菽婧 |
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| 作者单位： | 常州出入境检验检疫局,江苏常州213022 |
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| 基金项目： | 基金项目：江苏出入境检验检疫局科研项目（2013KJ21） |
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| 摘 要： | 建立了一种筛选皮革中邻苯二甲酸酯类增塑剂的方法。以丙酮为萃取溶剂，在40℃下微波萃取30min，萃取液经离子迁移谱检测，可实现对6种邻苯二甲酸酯的快速筛选。该方法简便快速，灵敏度高，各邻苯二甲酸酯检测低限在7～180mg，kg之间，满足欧盟REACH法规限量检测要求。
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| 关 键 词： | 皮革 邻苯二甲酸酯 离子迁移谱 筛选 REACH法规 |
Screening of Plasticizers in Leather Products by Ion Mobility Spectroscopy |
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| Authors: | WU Ze-ying LIU Hai-jun ZHU Jun XU Shu-jing |
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| Affiliation: | ( Changzhou Entry-Exit Inspection and Quarantine Bureau, Changzhou 213022, China) |
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| Abstract: | A screening method for the determination of phthalates plasticizers in leather using ion mobility spectroscopy is presented in this paper. The samples were extracted at 40℃ for 30 min by ultrasonic using acetone as the extracting solvent. The extract was analyzed by ion mobility spectroscopy, which enables the fast screening of 6 phthalates. The detection limit of each phthalate is between 7-180 mg/kg, which meets the determination requirement of REACH regulation. |
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| Keywords: | leather phthalates ion mobility spectroscopy screening REACH regulation |
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