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| 六味地黄滴心丸总糖含量测定 | |
| 引用本文： | 闫荟,杨立红,王苏会,张瑞淑.六味地黄滴心丸总糖含量测定[J].中国医药导报,2012,9(9):98-100. |
| 作者姓名： | 闫荟 杨立红 王苏会 张瑞淑 |
| 作者单位： | 1. 北京军区总医院药剂科,北京,100700 2. 北京军区药品器材供应站,北京,100700 3. 北京军区司令部门诊部,北京,100144 |
| 摘 要： | 目的建立六味地黄滴心丸总糖含量测定方法。方法以蒽酮-硫酸比色法,检测波长为625 nm,用葡萄糖为对照品对六味地黄滴心丸中总糖的含量进行测定。结果葡萄糖对照品溶液的线性范围为0.005 4～0.026 8 mg/mL（r=0.999 8）,平均回收率为98.30%。结论本研究确定的方法简便,可靠,准确,可用于六味地黄滴心丸中总糖的含量测定。 |
| 关 键 词： | 六味地黄滴心丸 总糖 蒽酮-硫酸法 |
The determination of total polysaccharides in Liuwei Dihuang Dropping Core Pills |
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| YAN Hui , YANG Lihong , WANG Suhui , ZHANG Ruishu.The determination of total polysaccharides in Liuwei Dihuang Dropping Core Pills[J].China Medical Herald,2012,9(9):98-100. | |
| Authors: | YAN Hui YANG Lihong WANG Suhui ZHANG Ruishu |
| Affiliation: | 1.Department of Pharmacy,the General Hospital of Beijing Millitry Region,Beijing 100700,China;2.Supply Station for Drug and Instrument,Beijing Millitry Region,Beijing 100700,China;3.The Outpatient Department of Beijing Military Command,Beijing 100144,China |
| Abstract: | Objective To establish the ultraviolet method for the determination of total polysaccharides in Liuwei Dihuang Dropping Core Pills.Methods Determination of total polysaccharide in Liuwei Dihuang Dropping Core Pills was carried out by anthrone-sulfuric acid colorimetric method with glucose as the standard at the wavelength of 625 nm.Results Calibration curve showed good linear regression(r = 0.999 8) with the range of 0.005 4-0.026 8 mg/mL.The average recovery was 98.30%.Conclusion The method in research is simple,reliable,accurate and can be used to determination of total polysaccharides in Liuwei Dihuang Dropping Core Pills. |
| Keywords: | Liuwei Dihuang Dropping Core Pills Total polysaccharides Anthrone-sulfuric acid colorimetric method |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |
