| 木香槟榔丸的质量标准研究 |
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| 引用本文： | 郭伟英,陈莹.木香槟榔丸的质量标准研究[J].中国药房,2011(43):4095-4097. |
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| 作者姓名： | 郭伟英 陈莹 |
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| 作者单位： | 辽宁医学院,锦州市121001 |
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| 摘 要： | 目的:建立木香槟榔丸的质量标准。方法:采用薄层色谱(TLC)法对制剂中的木香、槟榔、三棱、香附、莪术进行定性鉴别;采用高效液相色谱法测定制剂中盐酸小檗碱的含量。结果:TLC斑点明显、专属性强、重现性好,阴性对照无干扰;盐酸小檗碱进样量在0.320～1.600μg范围内与峰面积积分值呈良好线性关系(r=0.9997),平均回收率为99.29%,RSD=1.26%(n=6)。结论:所建标准可用于木香槟榔丸的质量控制。
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| 关 键 词： | 木香槟榔丸 薄层色谱法 高效液相色谱法 质量标准 |
Study on Quality Standard of Muxiang Binglang Pills |
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| GUO Wei-ying,CHEN Ying.Study on Quality Standard of Muxiang Binglang Pills[J].China Pharmacy,2011(43):4095-4097. |
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| Authors: | GUO Wei-ying CHEN Ying |
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| Affiliation: | (Liaoning Medical College, Jinzhou 121001, China) |
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| Abstract: | OBJECTIVE： To establish the quality standard for Muxiang binglang pills. METHODS： Aucklandia lappa, Areca catechu, Sparganium stoloniferum, Cyperus rotundus and Curcumae Rhizoma were identified by TLC. The contents of berberine hydrochloride in Muxiang binglang pills were determined by HPLC. RESULTS： The characteristic identification by TLC was distinctive, highly specific, reproducible, and free from the interference of the negative control substance. The linear range of berberine hydrochloride was 0.320-1.600 μg（r=0.999 7） with an average recovery rate of 99.29% （RSD=1.26% ,n=6）. CONCLUSION： The established standard is suitable for the quality control of Muxiang binglang pills. |
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| Keywords: | Muxiang binglang pills TLC HPLC Quality standard |
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