| 静电纺PLA微/纳米纤维膜的浸润性能研究 |
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| 引用本文： | 李常胜,李从举,付中玉,常敏,李小宁.静电纺PLA微/纳米纤维膜的浸润性能研究[J].合成纤维工业,2007,30(4):5-7. |
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| 作者姓名： | 李常胜 李从举 付中玉 常敏 李小宁 |
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| 作者单位： | 1. 北京服装学院材料工程学院,北京,100029
2. 北京市服装材料研究开发与评价重点实验室,北京,100029 |
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| 基金项目： | 教育部新世纪优秀人才支持计划资助(NCET-05-0204)，国家自然科学基金项目(50503001)，北京市自然科学基金项目北京市教委科技发展计划项目(KZ200510012010)。 |
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| 摘 要： | 采用静电纺丝技术制备聚乳酸(PLA)微/纳米纤维膜,研究了其可纺性、浸润性能及结构。结果表明:以二氯甲烷为溶剂的PLA电纺丝溶液,当PLA质量分数为7%时,可纺出纤维直径为280～690 nm的PLA微/纳米纤维膜。PLA微/纳米纤维膜与水的接触角为127.6°,高于PLA流延膜与水的接触角107.7°;红外光谱分析表明,PLA微/纳米纤维膜的分子组成没有发生变化;X光电子能谱测试表明PLA微/纳米纤维膜的表面碳氧含量比高于PLA流延膜,PLA微/纳米纤维膜的疏水性得到提高。
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| 关 键 词： | 聚乳酸 静电纺丝 浸润性 流延膜 接触角 红外光谱 X光电子能谱 |
| 文章编号： | 1001-0041（2007）04-0005-03 |
| 修稿时间： | 2006-10-18 |
Study on immersion behavior of electrospun PLA micro- and nano- fiber membranes |
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| Li Changsheng,Li Congju,Fu Zhongyu,Chang Min,Li Xiaoning.Study on immersion behavior of electrospun PLA micro- and nano- fiber membranes[J].China Synthetic Fiber Industry,2007,30(4):5-7. |
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| Authors: | Li Changsheng Li Congju Fu Zhongyu Chang Min Li Xiaoning |
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| Abstract: | Polylactic acid(PLA)micro-and nano-fiber membranes were prepared by electrospinning.Their spinnability,wet- tability and structure were studied.The results showed that the PLA micro-and nano-fiber membrane can be prepared with the diameter of 280-690 nm from PLA electrospinning solution with 7% PLA by mass fraction using methylene chloride as solvent. The contact angle between the fiber membrane and water was 127.6°,higher than the contact angle between cast film and water 107.7°.The infrared spectra showed that no transformation was observed in the molecular composition of PLA micro-and nano- fiber membrane.X-ray photoelectron spectroscopic analysis showed that the PLA micro-and nano-fiber membrane had higher carbon-and-oxygen ratio on the surface than PLA cast film,and the hydrophobicity of PLA micro-and nano-fiber membrane was improved. |
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| Keywords: | polylactic acid electrospinning immersion behavior cast film contact angle infrared spectrum X-ray photoelectron spectroscopy |
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