| 超高效液相色谱快速测定卷烟主流烟气中酚类化合物的研究 |
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| 引用本文： | 张婕,周淑平,耿召良,张长云,向章敏,李卫红,许冬青,赵瑞娟.超高效液相色谱快速测定卷烟主流烟气中酚类化合物的研究[J].化学工程师,2010(12):29-31,38. |
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| 作者姓名： | 张婕 周淑平 耿召良 张长云 向章敏 李卫红 许冬青 赵瑞娟 |
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| 作者单位： | 贵州省烟草科学研究所,测试中心,贵州,贵阳,550000 |
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| 基金项目： | 贵州省烟草公司科技计划项目 |
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| 摘 要： | 以卷烟主流烟气中酚类化合物的快速分析为内容,参照现有标准分析方法YC/T255-2008,研究了色谱条件由高效液相色谱(HPLC)变为超高效液相色谱(UPLC)的转换方法,建立了卷烟主流烟气中酚类化合物的UPLC快速分析方法。讨论了UPLC在实际应用中所遇到的问题及优缺点,为UPLC的应用开发提供参考。
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| 关 键 词： | 超高效液相色谱 色谱条件转化 酚类化合物 快速测定 |
An experimental study on rapid analysis of phenolic compounds in mainstream cigarette smoke by ultra performance liquid chromatography |
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| ZHANG Jie,ZHOU Shu-ping,GENG Zhao-liang,ZHANG Chang-yun,XIANG Zhang-min,LI Wei-hong,XU Dong-qing,ZHAO Rui-juan.An experimental study on rapid analysis of phenolic compounds in mainstream cigarette smoke by ultra performance liquid chromatography[J].Chemical Engineer,2010(12):29-31,38. |
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| Authors: | ZHANG Jie ZHOU Shu-ping GENG Zhao-liang ZHANG Chang-yun XIANG Zhang-min LI Wei-hong XU Dong-qing ZHAO Rui-juan |
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| Affiliation: | (Test Center,Guizhou Tobacco Science Institute,Guiyang 550000,China) |
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| Abstract: | A rapid method for the simultaneous separation and quantitation ofphenolic compounds in mainstream cigarette smoke has been developed by studing the conversion of chromato-graphic conditions from HPLC（YC/T 255-2008 standard method） to ultraperformance liquid chromatography system（UPLC）.An experimental design was carried out and discussed to achieve the best elution gradient for separation of all the studied compounds with the best possible peak resolution and in the shortest possible analysis time. |
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| Keywords: | UPLC conversion of chromatographic condition phenolic compounds rapid analysis |
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