| (E+Z)-2-[2-(4-N′-甲基-N′-甲烷磺酰基苯)-1-(4-氟苯)二苯甲酮基]-N-芳基-联氨羰草酰胺衍生物的合成 |
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| 引用本文： | 刘永榜,孔小林,彭伟立,沈德隆,邢家华,陈杰,夏旭建.(E+Z)-2-[2-(4-N′-甲基-N′-甲烷磺酰基苯)-1-(4-氟苯)二苯甲酮基]-N-芳基-联氨羰草酰胺衍生物的合成[J].浙江化工,2010,41(7):1-3. |
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| 作者姓名： | 刘永榜 孔小林 彭伟立 沈德隆 邢家华 陈杰 夏旭建 |
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| 作者单位： | 1. 浙江工业大学农药研究所,杭州,310014
2. 浙江省化工研究院有限公司,浙江,杭州,310023 |
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| 摘 要： | 为了寻求新的含缩氨基脲先导化合物,以对硝基苯甲酰氯,氟代苯,甲烷磺酰氯,水合肼、苯基异氰酸酯等为原料合成得到一类新的(E+Z)-2-2-(4-N′-甲基-N′-甲烷磺酰基苯)-1-(4-氟苯)二苯甲酮基]-N-芳基-联氨羰草酰胺衍生物。对所得化合物结构均经1HNMR和MS表征。
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| 关 键 词： | 二苯甲酮腙 缩氨基脲 合成 杀虫剂 |
Synthesis of (E+Z)-2-[2-(4-N'-methyl -N'- methanesulfonyl phenyl)-1-(4-fluorophenyl)Benzophenone]-N- aryl- hydrazine Carbonyl Oxamide Derivatives |
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| LIU yong-bang,KONG xiao-lin,PENG wei-li,SHEN de-long,XING jia-hua,CHEN jie,XIA xu-jian.Synthesis of (E+Z)-2-[2-(4-N'-methyl -N'- methanesulfonyl phenyl)-1-(4-fluorophenyl)Benzophenone]-N- aryl- hydrazine Carbonyl Oxamide Derivatives[J].Zhejiang Chemical Industry,2010,41(7):1-3. |
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| Authors: | LIU yong-bang KONG xiao-lin PENG wei-li SHEN de-long XING jia-hua CHEN jie XIA xu-jian |
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| Affiliation: | LIU yong-bang, KONG xiao-lin,PENG wei-li, SHEN de-long, XING jia-hua,CHEN jie, XlA xu-jian (1.Zhejiang University of Technology, Hangzhou 310014,China; 2.Zhejiang Chemical Industry Research Institute Co.,Ltd. Hangzhou 310023,China) |
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| Abstract: | In order to find new semicarbazone lead compounds, （E ＋Z）-2-2-（4-N＇-methyl -N＇- methanesulfonyl phenyl）-1-（4- fluorophenyl）Benzophenone]-N- aryl- hydrazine carbonyl oxamide derivatives were synthesized by 4-nitrobenzoyl chloride, fluorobenzene, methanesulfuryl chloride,hydrazine hydrate, phenylisoeyanates,etc. The structures of the products were characterized by ^1H NMR and MS. |
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| Keywords: | benzophenonehydrazone semiearbazone synthesis pesticide |
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