| 气相色谱法测定不同厂家复方丹参片中冰片含量 |
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| 引用本文： | 李冬梅,刘永利,袁浩.气相色谱法测定不同厂家复方丹参片中冰片含量[J].中国药业,2010,19(19):30-31. |
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| 作者姓名： | 李冬梅 刘永利 袁浩 |
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| 作者单位： | 河北省药品检验所,河北,石家庄,050011 |
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| 摘 要： | 目的建立复方丹参片中冰片的含量测定方法,并对不同厂家的样品进行比较。方法采用DB-WAX毛细管柱（30 m×0.53 mm,1μm）,FID检测器,乙酸乙酯为溶剂。结果平均加样回收率为99.31%,RSD为1.12%（n=9）。结论所用方法操作简便、重现性好、适用范围广,可作为复方丹参片中冰片的含量测定方法。
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| 关 键 词： | 复方丹参片 含量测定 气相色谱法 冰片 |
Determination of Borneol in Compound Danshen Tablets of Different Factories by GC |
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| Li Dongmei,Liu Yongli,Yuan Hao.Determination of Borneol in Compound Danshen Tablets of Different Factories by GC[J].China Pharmaceuticals,2010,19(19):30-31. |
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| Authors: | Li Dongmei Liu Yongli Yuan Hao |
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| Affiliation: | (Hebei Provincial Institute for Drug Control,Shijiazhuang,Hebei,China 050011) |
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| Abstract: | Objective To establish a capillary GC method for the determination of borneol in Compound Danshen Tablets and to compare the products made by different factories.Methods The DB-WAX capillary column（30 m × 0.53 mm,1 μm） was used with FID as detector and acetoacetate as solvent.Results The average recovery rate was 99.31%,RSD was 1.12%.Conclusion The method is simple,repro-ducible and applicable to a wide range,which can be used for the determination of borneol in Compound Danshen Tablets. |
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| Keywords: | Compound Danshen Tablets content determination GC borneol |
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