| 乳疾灵合剂质量标准研究 |
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| 引用本文： | 王明霞,李伟,侯娟,杜文力,朱敬山.乳疾灵合剂质量标准研究[J].中国药房,2006,17(16):1252-1254. |
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| 作者姓名： | 王明霞 李伟 侯娟 杜文力 朱敬山 |
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| 作者单位： | 河北医科大学第四医院,石家庄市,050011 |
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| 摘 要： | 目的:建立乳疾灵合剂的质量标准。方法:采用薄层色谱法对乳疾灵合剂中白芍、淫羊藿、丹参进行定性鉴别;采用高效液相色谱法测定白芍中主要成分芍药苷的含量。结果:供试品色谱中,在与白芍、淫羊藿、丹参对照药材相应的位置上,分别显相同颜色的斑点;芍药苷检测浓度在80~1280μg/ml范围内与峰面积积分值线性关系良好(r=0·9997),平均回收率为99·4%(RSD=1·8%)。结论:本方法简便、准确,可用于乳疾灵合剂的质量控制。
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| 关 键 词： | 乳疾灵合剂 高效液相色谱法 薄层色谱法 白芍 淫羊藿 丹参 芍药苷 质量标准 |
| 文章编号： | 1001-0408(2006)16-1252-03 |
| 收稿时间： | 09 28 2005 12:00AM |
| 修稿时间： | 02 21 2006 12:00AM |
Study on Quality Standard of Rujiling Mixture |
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| WANG Mingxia,LI Wei,HOU Juan,DU Wenli,ZHU Jingshan.Study on Quality Standard of Rujiling Mixture[J].China Pharmacy,2006,17(16):1252-1254. |
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| Authors: | WANG Mingxia LI Wei HOU Juan DU Wenli ZHU Jingshan |
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| Affiliation: | The Forth Hospital of Hebei Medical University, Shijiazhuang 050011, China |
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| Abstract: | OBJECTIVE:To establish the quality standard of Rujiling mixture.METHODS:Identification of Radix paeo-niae alba,Herba epimedii and Radix salviae miltiorrhizae was carried out by TLC;and the content of peoniflorin,the principal component in Radix paeoniae alba,was determined by HPLC.RESULTS:In the chromatography of samples,the same-colored speckles appeared at the corresponding positions of the reference substances of Radix paeoniae alba,Herba epimedii and Radix salviae miltiorrhizae.The linear range of peoniflorin was80～1280μg/mL(r=0.9997),and the average recovery was99.4%(RSD=1.8%).CONCLUSION:The method is simple,accurate,and suitable for the quality control of Rujiling mixture. |
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| Keywords: | Rujiling mixture HPLC TLC Radix paeoniae alba Herba epimedii Radix salviae mihiorrhizae Peoniflorin Quality standard |
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