| 单N－乙酸取代N_2O_2大环配体及其过渡金属配合物的合成与性质的研究 |
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| 引用本文： | 谢復新,田玉鹏,许志强,倪诗圣.单N－乙酸取代N_2O_2大环配体及其过渡金属配合物的合成与性质的研究[J].化学试剂,1994(2). |
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| 作者姓名： | 谢復新 田玉鹏 许志强 倪诗圣 |
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| 作者单位： | 安徽大学化学系 |
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| 摘 要： | 首次合成了一个新的单Ｎ－乙酸取代Ｈ_２Ｏ_２大环配体１，１２－二氮杂－３，４：９，１０－二苯并－５，８－二氧杂环十五烷－Ｎ－乙酸（ＨＬ）并制备了其过渡金属配合物。用红外光谱、元素分析、原子吸收、核磁共振及质谱等方法进行了表征。
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| 关 键 词： | 单N－乙酸取代氮氧杂大环，合成，过渡金属配合物 |
Synthesis and characterization of a new mono-N-acetic acid substituted N_2O_2 macrocycle and its complexes with transition metals |
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| Xie Fuxin,Tian Yupeng,Xu Zhiqiang,Ni Shisheng.Synthesis and characterization of a new mono-N-acetic acid substituted N_2O_2 macrocycle and its complexes with transition metals[J].Chemical Reagents,1994(2). |
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| Authors: | Xie Fuxin Tian Yupeng Xu Zhiqiang Ni Shisheng |
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| Abstract: | A new mono-N-acetic acid substituted N_2O_2 macrocycle,1, 12-diaza-3,4:9,10-dibenzo-5,8-dioxacyclopentadecane-N-acetic acid(HL)and its transition metal complexes are reported.They have been characterized by elemental analysis,A.A.,IR,HNMR and mass spectrometry. |
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| Keywords: | mono-N-acetic acid substituted N_2O_2 macrocycle synthesis transition metal complexes |
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