| 乙酸对甲苯酚酯的合成工艺研究 |
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| 引用本文： | 许国兵,王树清,高崇.乙酸对甲苯酚酯的合成工艺研究[J].精细石油化工进展,2009,10(8):50-51,55. |
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| 作者姓名： | 许国兵 王树清 高崇 |
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| 作者单位： | 1. 江苏安泰安全技术有限公司,南通,226007
2. 南通大学化学化工学院,南通,226007 |
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| 摘 要： | 以乙酰氯和对甲苯酚为原料合成了乙酸对甲苯酚酯，考察了反应温度、反应时间、原料配比等对合成反应的影响，确定了乙酸对甲苯酚酯的最佳合成工艺条件：反应温度40℃，反应时间7h，n（对甲苯酚）：n（乙酰氯）=1：1．5；乙酸对甲苯酚酯的收率可达94．95％，产品纯度达98．5％以上。
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| 关 键 词： | 乙酸对甲苯酚酯 乙酰氯 对甲苯酚 合成工艺 |
Study on Synthesis of p-Cresyl Acetate |
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| Xu Guobing,Wang Shuqing,Gao Chong.Study on Synthesis of p-Cresyl Acetate[J].Advances in Fine Petrochemicals,2009,10(8):50-51,55. |
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| Authors: | Xu Guobing Wang Shuqing Gao Chong |
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| Affiliation: | 1. Jiangsu Antai Safety Technology Co. Ltd. ,Nantong 226007 ; 2. College of Chemistry and Chemical Engineering, Nantong University, Nantong 226007) |
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| Abstract: | p- Cresyl acetate was synthesized with acetyl chloride and p -cresol as materials. The effects of reaction temperature, reaction time and material ratio on the synthesis were studied. The optimum synthesis condition was determined as follows： reaction temperature was 40 ℃, reaction time was 7 h, n（p -cresol）： n（acetyl chloride） was 1： 1.5. The yield ofp -cresyl acetate was up to 94.95%. The purity of the product was over 98.5%. |
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| Keywords: | p -cresyl acetate acetyl chloride p -cresol synthsis process |
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