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高体积分数的 SiCp/Al复合材料的 SPS致密化机理研究
引用本文:杨梅君,张东明,张联盟,顾晓峰.高体积分数的 SiCp/Al复合材料的 SPS致密化机理研究[J].无机材料学报,2007,22(4):695-700.
作者姓名:杨梅君  张东明  张联盟  顾晓峰
作者单位:武汉理工大学,材料复合新技术国家重点实验室,武汉,430070
摘    要:运用放电等离子烧结(SPS)技术制备出体积分数达60%,致密度达99%的SiCp/Al复合材料.从烧结工艺的控制及电场的影响两方面对SPS烧结SiC,/Al复合材料的机理进行了研究,认为SPS烧结SiCp/Al复合材料的致密化过程主要依靠烧结温度、压力及升温速率的合理搭配,使Al熔融粘结SiC颗粒,而又不溢出模具;烧结过程中未发现明显的放电现象,可能由于电场太弱不足以引发放电.

关 键 词:放电等离子烧结  SiCp/Al复合材料  烧结工艺  电场
文章编号:1000-324X(2007)04-0695-06
收稿时间:2006-7-28
修稿时间:2006-07-28

Consolidating Mechanism of High Volume Fraction of SiCp/Al Composites by SPS
YANG Mei-Jun,ZHANG Dong-Ming,ZHANG Lian-Meng,GU Xiao-Feng.Consolidating Mechanism of High Volume Fraction of SiCp/Al Composites by SPS[J].Journal of Inorganic Materials,2007,22(4):695-700.
Authors:YANG Mei-Jun  ZHANG Dong-Ming  ZHANG Lian-Meng  GU Xiao-Feng
Affiliation:State Key Laboratory of Advanced Technology for Materials Synthesis and Processing, Wuhan University of Technology, Wuhan 430070, China
Abstract:60vol%SiCp/Al composites with high relative density of 99% were fabricated by spark plasma sintering (SPS). The consolidating mechanism of SiCp/Al composites by SPS was analyzed on two aspects: (1) the adjustment of sintering parameters; (2) the effect of electric field. The results indicate that the consolidating procedure of SiCp/Al composites by SPS is mainly dependent on the proper adjustment of temperature, pressure and heating-rate which make Al melt and adhere SiC particles without spraying out of the graphite dies; no obvious spark appears during the sintering, which may result from the weak electric field.
Keywords:SPS  SiCp/Al composites  sintering parameter  electric field
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