| 固体酸催化合成环已酮1,2-丙二醇缩酮进展 |
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| 引用本文： | 俞善信,刘美艳,管仕斌,文瑞明.固体酸催化合成环已酮1,2-丙二醇缩酮进展[J].湖南文理学院学报(自然科学版),2006,18(3):28-34. |
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| 作者姓名： | 俞善信 刘美艳 管仕斌 文瑞明 |
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| 作者单位： | 湖南师范大学,化学化工学院,湖南,长沙,410081;湖南城市学院,化学与环境工程系,湖南,益阳,413000 |
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| 基金项目： | 湖南省教育厅科研基金资助项目(01C022) |
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| 摘 要： | 评述了对甲苯磺酸、氨基磺酸、强酸性阳离子交换树脂、六水三氯化铁、二水氯化亚锡、硫酸铜、水合硫酸铁、十二水合硫酸铁铵、硫酸钛、四水硫酸铈、铌酸、树脂固载Lewis酸、一水硫酸氢钠、碘、固体超强酸、杂多酸、分子筛和维生素C等催化剂催化合成环已酮1,2-丙二醇缩酮的实验结果.建议对近年来开发的有应用前景的催化剂进行扩大试验与筛选.
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| 关 键 词： | 环已酮1 2-丙二醇缩酮 合成 固体酸 催化 |
| 文章编号： | 1672-6146（2006）03-0028-07 |
| 收稿时间： | 2006-03-18 |
| 修稿时间： | 2006年3月18日 |
Progress on Synthesis of Cyclohexanone 1,2-propylene Ketal Catalyzed by Solid Acid |
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| YU Shan-xin,LIU Mei-yan,GUAN Shi-bin,WEN Rui-ming.Progress on Synthesis of Cyclohexanone 1,2-propylene Ketal Catalyzed by Solid Acid[J].Journal of Hunan University of Arts and Science:Natural Science Edition,2006,18(3):28-34. |
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| Authors: | YU Shan-xin LIU Mei-yan GUAN Shi-bin WEN Rui-ming |
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| Abstract: | It was reviewed that cyclohexanone 1,2-propy- lene ketal was catalytic synthesized of by the ketalization of cyclohexanone with 1,2-proplene glycol, including the experi- mental results of p-toluene sulfonic acid, amino sulfonic acid, strongly acidic cationic exchange resin, ferric chloride hexahydrate, stannous chloride dihydrate, copper sulfate, ferric sulfate hydrate, ammonium ferric sulfate dodecahydrate, titanium sulfate,cerium sulfate tetrahydrate, niobic acid, resin support Lewis acid, sodium bisulfate monohydrate, Iodine, solid super acid, heteropdy acid, molecular sieve and vitamin C etc. al. It was suggested that the experiment and selection of promising catalyst developed in the recet years should be enhanced. |
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| Keywords: | cyclohexanone 1 2-proplene ketal synthesis solid acid catalysis |
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