麻仁合剂质量标准的研究 |
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引用本文: | 雪秦岚,张华,赵宏科.麻仁合剂质量标准的研究[J].中国药品标准,2004,5(1):54-56. |
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作者姓名: | 雪秦岚 张华 赵宏科 |
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作者单位: | 陕西宝鸡华西制药有限公司,宝鸡,721001 |
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摘 要: | 目的:控制麻仁合剂的质量.方法:采用薄层色谱法鉴别麻仁合剂中大黄素、大黄酚、厚朴酚;采用高效液相色谱法测定芍药苷的含量.结果:定性鉴别斑点圆整,分离度好.含量测定芍药苷平均加样回收率为98.49%,RSD为1.81%.结论:方法简便、准确、重现性好,可用于麻仁合剂的质量控制.
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关 键 词: | 麻仁合剂 质量标准 薄层色谱法 高效液相色谱法 大黄素、大黄酚、厚朴酚、芍药苷 |
Study on Quality Standard for maren Mixture |
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Authors: | Xue Qinlan Zhang Hua and Zhao Hongke |
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Affiliation: | Bao ji Huaxi pharmaceutical Co., Ltd. Shannxi 721001, China;Bao ji Huaxi pharmaceutical Co., Ltd. Shannxi 721001, China;Bao ji Huaxi pharmaceutical Co., Ltd. Shannxi 721001, China |
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Abstract: | AIM:To control the quality of Maren Mixture,Methods:Emodin,Chrysophanol and magnolol of maren Mixture were identified by TLC. Paeonifiorin of the Mixture was determined by HPLC. Results:The studies showed that spot of naringoside on TLC can be well separated. The average recovery rate of the spiked sample was 98- 49%and RSD was 1. 85%. Conclusion: The method established was simple,accurate and with good reproducibility. The method can be used for quality control of Maren Mixture |
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Keywords: | Maren Mixture quality standard TLC HPLC emodin chrysophanol magnolol paeoniflorin |
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