| 1,2,4-三嗪类化合物的研究ⅩⅦ——3-甲硫基-5-羟基-1,2,4-三嗪的不正常对甲苯磺酰化产物的质谱鉴定及结构研究 |
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| 引用本文： | 程铁明,韩梅,胡长风,蔡孟深.1,2,4-三嗪类化合物的研究ⅩⅦ——3-甲硫基-5-羟基-1,2,4-三嗪的不正常对甲苯磺酰化产物的质谱鉴定及结构研究[J].质谱学报,1992(2). |
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| 作者姓名： | 程铁明 韩梅 胡长风 蔡孟深 |
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| 作者单位： | 北京医科大学药学院
(程铁明，韩梅，胡长风)，北京医科大学药学院(蔡孟深) |
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| 摘 要： | 运用质谱分析等手段,对3-甲硫基-5-羟基-1,2,4-三嗪的对甲苯磺酰化反应的产物进行系统鉴定,并通过高分辨质谱确定其新化合物为N-6-(3-甲硫基-5-负氧基-1,2,4-三嗪基)]吡啶内鎓盐。
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| 关 键 词： | 1 2 4-三嗪类化合物 质谱 |
Chemistry of 1,2,4-Triazines XVII Study on Mass Spectrometry and Structuresof Products from an Anomalous Tosylatjon of 3-Methylthio-5-hydroXy-1,2,4-triazine |
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| Cheng Ticming,Han Mei,Hu Changfeng,Cai Mengshen.Chemistry of 1,2,4-Triazines XVII Study on Mass Spectrometry and Structuresof Products from an Anomalous Tosylatjon of 3-Methylthio-5-hydroXy-1,2,4-triazine[J].Journal of Chinese Mass Spectrometry Society,1992(2). |
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| Authors: | Cheng Ticming Han Mei Hu Changfeng Cai Mengshen |
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| Abstract: | A systematic studies on determination of the structure of products in tosylation of 3-methylthio-5-hydroxy-1,2,4-triazine by MS were reported. One of products is N-3-methylthio-5-oxy-1,2,4-triazin-6-yl pyridinium betaine by high resolution mass spectrometry. |
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| Keywords: | 1 2 4-Triazines Mass Spectrometry |
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