| 5-(对-羟基苯基)-10,15,20-三苯基卟啉的金属化及性质表征 |
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| 引用本文： | 单凝,郑文琦,法焕宝,王杏乔.5-(对-羟基苯基)-10,15,20-三苯基卟啉的金属化及性质表征[J].吉林大学学报(理学版),2007,45(2):283-287. |
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| 作者姓名： | 单凝 郑文琦 法焕宝 王杏乔 |
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| 作者单位： | 吉林大学 化学学院, 长春 130021 |
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| 摘 要： | 设计、 合成、 分离了5-(对羟基苯基)-10,15,20-三苯基卟啉化合物, 并合成其金属配合物. 通过元素分析, IR,UV-vis和1HNMR等方法确证了这些化合物的结构,给出了卟啉类配体与金属配合物的IR，UV-vis和1HNMR判据， 并对它们的热稳定性质进行了研究.
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| 关 键 词： | 金属卟啉 表征 差热热重 |
| 文章编号： | 1671-5489(2007)02-0283-05 |
| 收稿时间： | 2006-05-17 |
| 修稿时间： | 2006年5月17日 |
Metallization and Characterization of meso-5-(p-hydroxyphenyl)-10,15,20-triphenylporphyrin |
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| SHAN Ning,ZHENG Wen-qi,FA Huan-bao,WANG Xing-qiao.Metallization and Characterization of meso-5-(p-hydroxyphenyl)-10,15,20-triphenylporphyrin[J].Journal of Jilin University: Sci Ed,2007,45(2):283-287. |
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| Authors: | SHAN Ning ZHENG Wen-qi FA Huan-bao WANG Xing-qiao |
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| Affiliation: | College of Chemistry, Jilin University, Changchun 130021, China |
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| Abstract: | Different transition metalloporphyrins(Mn,Fe,Co,Ni,Cu,Zn) were prepared,purified and they were characterized by means of element analysis,IR,UV-vis and 1HNMR.The correlation between the structures of the compounds and their 1HNMR,IR,UV spectra was discussed and their specific spectra were explained. The thermostabilities of the compounds were studied with the aid of TGA-TDA. |
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| Keywords: | metalloporphyrins characterization TGA-TDA thermogram |
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