| 1,4-二巯基苏醇的高效液相色谱分析 |
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| 引用本文： | 高永民,李辉,陈美玲,王树伟.1,4-二巯基苏醇的高效液相色谱分析[J].精细化工中间体,2002,32(6):54-54,57. |
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| 作者姓名： | 高永民 李辉 陈美玲 王树伟 |
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| 作者单位： | 1. 河北威远集团,石家庄,050031
2. 石家庄金鱼涂料集团,050051 |
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| 摘 要： | 采用C18 反相柱和紫外吸收检测器 ,以甲醇 +乙腈 +水作流动相 ,对 1,4 二巯基苏醇进行液相色谱分离 ,外标法定量。方法线性范围宽、精密度好、准确度高。
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| 关 键 词： | 1 4二巯基苏醇 液相色谱 分析 |
| 文章编号： | 1009-9212(2002)06-0054-01 |
Analysis of 1,4-Dithiothreitol by HPLC |
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| GAO Yong-min,et al..Analysis of 1,4-Dithiothreitol by HPLC[J].Fine Chemical Intermediates,2002,32(6):54-54,57. |
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| Authors: | GAO Yong-min |
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| Abstract: | The quantitative analysis of 1,4-Dithiothreitol by HPLC on C 18 reversed phase column with UV-absorbance detector and mobile phase of methol + acetonitrile + water. The calibration curve was linear in the range of 0.01～2.0 g/L, the standard deviation was 0.19, the coefficient of variation was 0.20% and the recovery was 97.8%～102.0%. |
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| Keywords: | Dithiothreitol HPLC analysis |
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