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由60 MeV18O8+离子轰击UO2(NO3)2制备稀土多重示踪剂
引用本文:温永红,秦芝,刘伟生.由60 MeV18O8+离子轰击UO2(NO3)2制备稀土多重示踪剂[J].兰州大学学报(自然科学版),2002,38(1):58-61.
作者姓名:温永红  秦芝  刘伟生
作者单位:1. 兰州大学,化学化工学院,甘肃,兰州,730000
2. 中国科学院,兰州近代物理研究所,甘肃,兰州,730000
基金项目:国家自然科学基金资助项目 (2 0 0 710 15 )
摘    要:用60MeV^18O^8 离子照射UO2(NO3)2,靶子物质溶于王水,经(ψ=20%TBP-C6H6萃取,浓直酸沉淀,0.4mol/L的HDEHP-n-heptane萃取,8mol/L的HCl反萃,得到了含有12种稀土元素的18种放射性核素的无载体多重示踪剂。

关 键 词:稀土多重示踪剂  溶剂萃取法  放射化学分析技术  60MeV  中能重离子  UO2(NO3)2  氧离子轰击
文章编号:0455-2059(2002)01-0058-04
修稿时间:2001年5月16日

Preparation of a rare earth multitracer solution from UO2(NO3)2 irradiated by 60 MeV/nucleon 18O8+ ions
WEN Yong-hong ,QIN Zhi ,LIU Wei-sheng.Preparation of a rare earth multitracer solution from UO2(NO3)2 irradiated by 60 MeV/nucleon 18O8+ ions[J].Journal of Lanzhou University(Natural Science),2002,38(1):58-61.
Authors:WEN Yong-hong  QIN Zhi  LIU Wei-sheng
Affiliation:WEN Yong-hong 1,QIN Zhi 2,LIU Wei-sheng 1
Abstract:UO 2(NO 3) 2 as a target was irradiated with a 60 MeV/nucleon 18O 8 ion beam,and dissolved in aqua regia.The uranyl was removed from 6 mol/L HNO 3 by means of solvent extraction with TBP in benzene,and the barium was separated by BaCl 2 precipitation.A 0.4 mol/L solution of HDEHP in n-heptane was used for extraction of rare earth elements from 0.5 mol/L HCl,and back extraction was carried out with an equal volume of 8 mol/L HCl after the organic phase was diluted by adding the same volume of n-heptane.A carrier-free multitracer solution containing 18 radionuclides of 12 rare earth elements was prepared.
Keywords:rare earth  multitracer  solvent extraction
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