| 硫酸氢钠催化合成乙酸异丙酯 |
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| 引用本文： | 徐常龙,柳闽生,蔡水莲,王贤亮.硫酸氢钠催化合成乙酸异丙酯[J].化工中间体,2005(8):22-23,4. |
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| 作者姓名： | 徐常龙 柳闽生 蔡水莲 王贤亮 |
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| 作者单位： | 江西省九江学院化学系,332000 |
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| 摘 要： | 以自制的硫酸氢钠为催化剂，以冰乙酸与异丙醇为原料合成了乙酸异丙酯。最佳反应条件为：以0.2摩尔异丙醇为基准，醇酸摩尔比为1：1.5，催化剂用量为1.2g，反应温度控制在回流温度。酯收率最高可达到75.2％。
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| 关 键 词： | 硫酸氢钠 催化酯化 乙酸异丙酯 |
| 文章编号： | 1006-253x（2005）08-005-22-2 |
Synthesis of Isopropyl acetate Using sodium Bisulfate as catalyst |
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| Authors: | XU Changlong Liu Minsheng Cai Shuilian Wang Xianliang |
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| Abstract: | Isopropyl acetate, was synthesized using sodium bisulfate made by ourselves as catalyst, with acetic acid and Isopropyl as materials. The best condition of reaction is: if, on the basis of 0.2mol isopropyl, the mass of catalyst reaching 1.3g, the temperature of reaction controlled about 95, the rate of isopropyl and acetic acid is 1 to 1.5, the highest yield of the reaction can reach75.2%. |
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| Keywords: | sodium bisulfate catalysis isopropyl acetate |
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