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The Influence of the Amount of Fluoride Catalyst on the Morphological Properties of the Anilinepropylsilica Xerogel Prepared in Basic Medium
Authors:Flávio A Pavan  Sidinei A Gobbi  Celso C Moro  Tania MH Costa  Edilson V Benvenutti
Affiliation:(1) LSS—Laboratório de Sólidos e Superficies, Instituto de Quimica, UFRGS, CP 15003, 915019-70 Porto Alegre, RS, Brazil
Abstract:Anilinepropylsilica hybrid powder was synthesized by a sol-gel route in basic medium using HF as catalyst. The effect of the amount of HF catalyst on the morphologies and on organic content was studied. The xerogels were characterized using FTIR, SEM and N2 adsorption-desorption isotherms. The increase in the HF quantity results in an slight increase in organic content and changes in the particle size, surface area and pore structure.
Keywords:amorphous materials  microporous materials  nanostructures  hybrid xerogels
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