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气相色谱-质谱法分析棕榈果脂肪酸组成
引用本文:沈丹玉,汤富彬,钟冬莲,倪张林,屈明华,莫润宏.气相色谱-质谱法分析棕榈果脂肪酸组成[J].中国粮油学报,2012,27(1):111-113,119.
作者姓名:沈丹玉  汤富彬  钟冬莲  倪张林  屈明华  莫润宏
作者单位:中国林业科学研究院亚热带林业研究所 国家林业局经济林产品质量检验检测中心(杭州),富阳,311400
基金项目:中央级公益性科研院所基本科研业务费专项资金(6151)
摘    要:采用索氏抽提法分别提取棕榈果肉和棕榈果仁中的油脂,以氢氧化钾—甲醇溶液对油脂进行甲酯化处理,用气相色谱-质谱(GC-MS)法分析。从棕榈果肉和棕榈仁的油脂中均分离并鉴定了9种脂肪酸,其中棕榈果肉中饱和脂肪酸质量分数为49.5%,主要有棕榈酸和硬脂酸,不饱和脂肪酸主要有油酸、亚油酸以及少量的亚麻酸和13,16-二十二碳二烯酸。棕榈仁中饱和脂肪酸80%以上,其中月桂酸质量分数达到41.5%,肉豆蔻酸和棕榈酸含量也较高,此外还含有少量的己酸、辛酸、癸酸和硬脂酸,不饱和脂肪酸有油酸和亚油酸。

关 键 词:棕榈果  棕榈仁  棕榈油  脂肪酸  气相色谱-质谱

Analysis of Fatty Acid Composition in Oil Palm Fruit by Chromatography-Mass Spectrometry
Shen Danyu , Tang Fubin , Zhong Donglian , Ni Zhanglin , Qu Minghua , Mo Runhong.Analysis of Fatty Acid Composition in Oil Palm Fruit by Chromatography-Mass Spectrometry[J].Journal of the Chinese Cereals and Oils Association,2012,27(1):111-113,119.
Authors:Shen Danyu  Tang Fubin  Zhong Donglian  Ni Zhanglin  Qu Minghua  Mo Runhong
Affiliation:Shen Danyu Tang Fubin Zhong Donglian Ni Zhanglin Qu Minghua Mo Runhong(Research Institute of Subtropical Forestry,Chinese Academy of Forestry, Quality Testing Center for Non-wood Forest Products of State Forestry Administration(Hangzhou),Fuyang 311400)
Abstract:Palm oil and palm kernel oil were extracted by a soxhlet extractor,and esterfied with potassium hydroxide-methanol.The fatty acid compositions were determined by gas chromatography-mass spectrometry.Nine fatty acids were identified and quantified respectively.The relative content of saturated fatty acids from palm oil was 49.5 %,and existing forms were mainly palmitic acid and stearic acid.The unsaturated fatty acids were constituted of oleic acid,linoleic acid,linolenic acid and cis-13,16-docosadienoic acid.The relative content of saturated fatty acids from palm kernel oil was more than 80,and lauric acid had the highest content obtained with content of 41.5% among them.The other main compositions were myristic acid,palmitic acid,hexanoic acid,octanoic acid,capric acid and stearic acid.Oleic acid and linoleic acid constituted the unsaturated fatty acids.
Keywords:oil palm fruit  palm kernel  palm oil  fatty acids  gas chromatography-mass spectrometry
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