| 吡啶环化合物的合成与结构表征 |
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| 引用本文： | 杨晓炯,乔妙杰,马晨,李彦奎.吡啶环化合物的合成与结构表征[J].山西化工,2014(2):5-7. |
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| 作者姓名： | 杨晓炯 乔妙杰 马晨 李彦奎 |
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| 作者单位： | 中国电子科技集团第三十三研究所; |
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| 摘 要： | 以2,6-二甲基吡啶、正丁基锂为初始原料,在温和的条件下,经1倍正丁基锂去氢后与苯乙酮加成得到含N,O-二齿配体化合物2-(6-(CH3)C5H4N)CH2C(OH)(Ph)CH3],应用1 H NMR技术对其进行了结构表征。
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| 关 键 词： | 吡啶环化合物 合成 表征 |
Synthesis and structural characterization of pyridine ring compounds |
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| YANG Xiao-jiong,QIAO Miao-jie,MA Chen,LI Yan-kui.Synthesis and structural characterization of pyridine ring compounds[J].Shanxi Chemical Industry,2014(2):5-7. |
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| Authors: | YANG Xiao-jiong QIAO Miao-jie MA Chen LI Yan-kui |
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| Affiliation: | (The 33rd Institude of China Electronics Technology Group Corporation, Taiyuan Shanxi 030006, China) |
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| Abstract: | This research takes 2,6-dimethyl pyridine, n-butyl lithium as initial raw materials, which is dehydroed by double n- butyl lithium in mild conditions and mixed with acetophenone to get the compound 2-（6-（CH3 ）C5 H4 N）CH2 C（OH）（Ph）CH3 ] containing N,O-bidentate ligand. This compound is characterized by 1H NMR technique. |
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| Keywords: | pyridine ring compounds synthesis characterization |
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