| 毛细管气相色谱法定量分析腐霉利 |
| |
| 引用本文： | 李兰春,张强,张耕,张桂齐,王硕,张武.毛细管气相色谱法定量分析腐霉利[J].化工中间体,2008,4(10):47-49. |
| |
| 作者姓名： | 李兰春 张强 张耕 张桂齐 王硕 张武 |
| |
| 作者单位： | 农业部农药质量监督检验测试中心,天津,天津,300061 |
| |
| 摘 要： | 采用DB-35石英毛细管色谱柱和FID检测器，以邻苯二甲酸二丁酯为内标物，在适宜的色谱条件下对腐霉利进行定量分析。色谱条件为柱箱温度220℃；进样口温度280℃，检测器温度280℃，气体流速为载气（N2）6mL／min，燃气（H2）30mL／min，助燃气（Air）300mL／min，分流比20：1。本方法的变异系数0．316％，平均回收率99．82％，线性相关系数为0．9999。
|
| 关 键 词： | 腐霉利 定量分析 毛细管气相色谱 |
Quantitative Analysis of Procymidone by Capillary Gas Chromatography |
| |
| Authors: | Li Lanehun Zhang Qiang Zhang Guiqi WangShuo Zhang Wu |
| |
| Affiliation: | Li Lanehun Zhang Qiang Zhang Guiqi WangShuo Zhang Wu (Supervise and Test Center for Pesticide of Ministry of Agriculture (Tianjin),Tianjin 300061,China) |
| |
| Abstract: | Quantitative analysis of Procymidone quantitation by using Dibutyl phthalate as internal standard with DB-35 Quartz capillary chromatographic column and FID detector in appropriate Chromatographic conditions. The chromatographic conditions is that Column temperature is 220℃, I injector temperature is 280℃,FID detector is used with temperature 280℃. The Gas flow rate is that Carrier gas （N2） is 6.0 mL/min, gas （H2） is 30 mL/min, air is 300 mL/min and split ratio is 20：1. The coefficient of variation was 0.316%, the average recovery was 99.82%, and the coefficient of linear correlation was 0.9999. |
| |
| Keywords: | procymidone quantitative analysis capillary gas chromatography |
| 本文献已被 维普 万方数据 等数据库收录！ |
|
